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Electrocatalytic activity of nano-sized Ebonex/Pt for underpotential deposition of hydrogen
(Trans Tech Publications Ltd, 2006)
The underpotential deposition of hydrogen was studied in 0.5 mol dm(-3) HClO4 solution on an electrode based on Ebonex-supported platinum electrocatalyst spread on rotation Au disk electrode (Ebonex/Pt). Pt catalyst was ...
Microstructural properties of PZT thin films deposited on LaNIQ 3-coated substrates
(Trans Tech Publications Ltd, 2007)
The modified polymeric precursor method (Pechini method) was successfully used for the preparation of epitaxial and polycrystalline ferroelectric Pb(Zr0.52Ti0.48)O3 (PZT) thin films. Films were deposited on LaNiO3 (LNO) - ...
Synthesis of pure and doped LaMnO3 powders from citrate precursors
(Trans Tech Publications Ltd, 2007)
In this work pure and doped LMO were prepared using modified Pechini method from lanthanum and manganese citrates. Lanthanum citrate was prepared starting from La2O3, while manganese citrate was prepared from Mn(NO3)(2). ...
Spectroscopic studies of SnO2 doped with Cr, Co or Nb
(Trans Tech Publications Ltd, 2003)
SnO2 ceramics doped with different amounts of Co, Cr or Nb were investigated using visible and infrared spectroscopy at room temperature. Based on the observed d-d transitions the valence states of incorporated dopants ...
Mechanochemical synthesis of CaTiO3 from CaCO3-TiO2 mixture
(Trans Tech Publications Ltd, 2004)
The synthesis of calcium titanate, CaTiO3, was performed by mechanical activation and thermal treatment. Milling for up to 360 minutes in a planetary ball mill mechanically activated an equimolar mixture of CaCO3 and TiO2 ...
Electrical characterization of the grain-boundary region of SnO2 varistors
(Trans Tech Publications Ltd, 2006)
The effect of Co, Cr and Nb on the electrical properties of the grain boundaries of SnO2-based varistors was investigated. The powders were prepared by the method of evaporation and decomposition of solutions and suspensions. ...
Application of the master sintering curve theory to non-isothermal sintering of BaTiO3 ceramics
(Trans Tech Publications Ltd, 2005)
In this paper a practical approach to the analysis of sintering of BaTiO3 using the Master Sintering Curve concept has been presented. Non-isothermal sintering of high-purity non-doped BaTiO3 ceramics was monitored using ...
The influence of mechanical activation on the stoichiometry and defect structure of a sintered ZnO-Cr2O3 system
(Trans Tech Publications Ltd, 2004)
Mixtures of starting ZnO and Cr2O3 powders in equimolar quantities were mechanically activated by grinding using a high energy vibro-mill for 0, 40 and 80 minutes. Qualitative X-ray diffraction analysis made after sintering ...