In this work pure and doped LMO were prepared using modified Pechini method from lanthanum and manganese citrates. Lanthanum citrate was prepared starting from La2O3, while manganese citrate was prepared from Mn(NO3)(2). Valence state of the manganese was controlled by adjusting pH value of the solution and confirmed by EPR and UV/VIS analysis. Thermal treatment conditions for preparation of LMO powders were determined from TG/DTA of dried precursors. XRD results confirmed that pure perovskite phase was successfully prepared in single LMO and Ca-doped LMO. SEM and measurements of specific surface area of the powders showed the existence of large agglomerates consisting of submicronic primary particles.
TY - JOUR
AU - Djuriš, K.
AU - Branković, Goran
AU - Branković, Zorica
AU - Bernik, Slavko
AU - Počuča-Nešić, Milica
AU - Poleti, Dejan
AU - Antić, B.
PY - 2007
UR - http://rimsi.imsi.bg.ac.rs/handle/123456789/218
AB - In this work pure and doped LMO were prepared using modified Pechini method from lanthanum and manganese citrates. Lanthanum citrate was prepared starting from La2O3, while manganese citrate was prepared from Mn(NO3)(2). Valence state of the manganese was controlled by adjusting pH value of the solution and confirmed by EPR and UV/VIS analysis. Thermal treatment conditions for preparation of LMO powders were determined from TG/DTA of dried precursors. XRD results confirmed that pure perovskite phase was successfully prepared in single LMO and Ca-doped LMO. SEM and measurements of specific surface area of the powders showed the existence of large agglomerates consisting of submicronic primary particles.
PB - Trans Tech Publications Ltd
T2 - Materials Science Forum
T1 - Synthesis of pure and doped LaMnO3 powders from citrate precursors
EP - 242
SP - 237
VL - 555
DO - 10.4028/0-87849-441-3.237
ER -
@article{
author = "Djuriš, K. and Branković, Goran and Branković, Zorica and Bernik, Slavko and Počuča-Nešić, Milica and Poleti, Dejan and Antić, B.",
year = "2007",
abstract = "In this work pure and doped LMO were prepared using modified Pechini method from lanthanum and manganese citrates. Lanthanum citrate was prepared starting from La2O3, while manganese citrate was prepared from Mn(NO3)(2). Valence state of the manganese was controlled by adjusting pH value of the solution and confirmed by EPR and UV/VIS analysis. Thermal treatment conditions for preparation of LMO powders were determined from TG/DTA of dried precursors. XRD results confirmed that pure perovskite phase was successfully prepared in single LMO and Ca-doped LMO. SEM and measurements of specific surface area of the powders showed the existence of large agglomerates consisting of submicronic primary particles.",
publisher = "Trans Tech Publications Ltd",
journal = "Materials Science Forum",
title = "Synthesis of pure and doped LaMnO3 powders from citrate precursors",
pages = "242-237",
volume = "555",
doi = "10.4028/0-87849-441-3.237"
}
Djuriš, K., Branković, G., Branković, Z., Bernik, S., Počuča-Nešić, M., Poleti, D.,& Antić, B.. (2007). Synthesis of pure and doped LaMnO3 powders from citrate precursors. in Materials Science Forum
Trans Tech Publications Ltd., 555, 237-242.
https://doi.org/10.4028/0-87849-441-3.237
Djuriš K, Branković G, Branković Z, Bernik S, Počuča-Nešić M, Poleti D, Antić B. Synthesis of pure and doped LaMnO3 powders from citrate precursors. in Materials Science Forum. 2007;555:237-242.
doi:10.4028/0-87849-441-3.237 .
Djuriš, K., Branković, Goran, Branković, Zorica, Bernik, Slavko, Počuča-Nešić, Milica, Poleti, Dejan, Antić, B., "Synthesis of pure and doped LaMnO3 powders from citrate precursors" in Materials Science Forum, 555 (2007):237-242,
https://doi.org/10.4028/0-87849-441-3.237 . .
