dc.creator | Branković, Zorica | |
dc.creator | Branković, Goran | |
dc.creator | Počuča-Nešić, Milica | |
dc.creator | Marinković-Stanojević, Zorica | |
dc.creator | Žunić, Milan | |
dc.creator | Luković Golić, Danijela | |
dc.creator | Tararam, R. | |
dc.creator | Cilense, Mario | |
dc.creator | Zaghete, M. A. | |
dc.creator | Jaglicic, Z. | |
dc.creator | Jagodic, M. | |
dc.creator | Varela, JA | |
dc.date.accessioned | 2022-04-05T14:57:04Z | |
dc.date.available | 2022-04-05T14:57:04Z | |
dc.date.issued | 2015 | |
dc.identifier.issn | 0272-8842 | |
dc.identifier.uri | http://rimsi.imsi.bg.ac.rs/handle/123456789/881 | |
dc.description.abstract | In this work single phase hexagonal YMnO3 powders were prepared starting from Y(CH3COO)(3)center dot xH(2)O, Mn(CH3COO)(2)center dot 4H(2)O, KMnO4 and KOH using methods of conventional (280 degrees C for 6 h) or microwave assisted hydrothermal synthesis (200 degrees C for 2 h) followed by calcination at 1200 degrees C for 2 h. According to FESEM analysis the calcined powders consisted of submicronic YMnO3 particles, which were uniform in shape and size. Ceramic samples were obtained by sintering the as-synthesized powders at 1400 degrees C for 2 h. XRD analysis confirmed the presence of the single phase hexagonal YMnO3. SEM analysis showed a dense and homogeneous microstructure with typical inter- and intra-grain cracks. Magnetic measurements indicated ferrimagnetic properties that were explained by non-stoichiometry of the obtained compound and an excess of manganese that was confirmed by ICP analysis. | en |
dc.publisher | Elsevier Sci Ltd, Oxford | |
dc.relation | info:eu-repo/grantAgreement/MESTD/Integrated and Interdisciplinary Research (IIR or III)/45007/RS// | |
dc.relation | Fundacao de Amparo a Pesquisa do Estado de Sao Paulo-FAPESPFundacao de Amparo a Pesquisa do Estado de Sao Paulo (FAPESP) [2011/00922-0] | |
dc.rights | restrictedAccess | |
dc.source | Ceramics International | |
dc.subject | Yttrium manganite | en |
dc.subject | Phase evolution | en |
dc.subject | Magnetic measurements | en |
dc.subject | Hydrothermal synthesis | en |
dc.title | Hydrothermally assisted synthesis of YMnO3 | en |
dc.type | article | |
dc.rights.license | ARR | |
dc.citation.epage | 14298 | |
dc.citation.issue | 10 | |
dc.citation.other | 41(10): 14293-14298 | |
dc.citation.rank | M21 | |
dc.citation.spage | 14293 | |
dc.citation.volume | 41 | |
dc.identifier.doi | 10.1016/j.ceramint.2015.07.060 | |
dc.identifier.scopus | 2-s2.0-84938125324 | |
dc.identifier.wos | 000362919900046 | |
dc.type.version | publishedVersion | |