In this work single phase hexagonal YMnO3 powders were prepared starting from Y(CH3COO)(3)center dot xH(2)O, Mn(CH3COO)(2)center dot 4H(2)O, KMnO4 and KOH using methods of conventional (280 degrees C for 6 h) or microwave assisted hydrothermal synthesis (200 degrees C for 2 h) followed by calcination at 1200 degrees C for 2 h. According to FESEM analysis the calcined powders consisted of submicronic YMnO3 particles, which were uniform in shape and size. Ceramic samples were obtained by sintering the as-synthesized powders at 1400 degrees C for 2 h. XRD analysis confirmed the presence of the single phase hexagonal YMnO3. SEM analysis showed a dense and homogeneous microstructure with typical inter- and intra-grain cracks. Magnetic measurements indicated ferrimagnetic properties that were explained by non-stoichiometry of the obtained compound and an excess of manganese that was confirmed by ICP analysis.
TY - JOUR
AU - Branković, Zorica
AU - Branković, Goran
AU - Počuča-Nešić, Milica
AU - Marinković Stanojević, Zorica
AU - Žunić, Milan
AU - Luković Golić, Danijela
AU - Tararam, R.
AU - Cilense, Mario
AU - Zaghete, M. A.
AU - Jaglicic, Z.
AU - Jagodic, M.
AU - Varela, JA
PY - 2015
UR - http://rimsi.imsi.bg.ac.rs/handle/123456789/881
AB - In this work single phase hexagonal YMnO3 powders were prepared starting from Y(CH3COO)(3)center dot xH(2)O, Mn(CH3COO)(2)center dot 4H(2)O, KMnO4 and KOH using methods of conventional (280 degrees C for 6 h) or microwave assisted hydrothermal synthesis (200 degrees C for 2 h) followed by calcination at 1200 degrees C for 2 h. According to FESEM analysis the calcined powders consisted of submicronic YMnO3 particles, which were uniform in shape and size. Ceramic samples were obtained by sintering the as-synthesized powders at 1400 degrees C for 2 h. XRD analysis confirmed the presence of the single phase hexagonal YMnO3. SEM analysis showed a dense and homogeneous microstructure with typical inter- and intra-grain cracks. Magnetic measurements indicated ferrimagnetic properties that were explained by non-stoichiometry of the obtained compound and an excess of manganese that was confirmed by ICP analysis.
PB - Elsevier Sci Ltd, Oxford
T2 - Ceramics International
T1 - Hydrothermally assisted synthesis of YMnO3
EP - 14298
IS - 10
SP - 14293
VL - 41
DO - 10.1016/j.ceramint.2015.07.060
ER -
@article{
author = "Branković, Zorica and Branković, Goran and Počuča-Nešić, Milica and Marinković Stanojević, Zorica and Žunić, Milan and Luković Golić, Danijela and Tararam, R. and Cilense, Mario and Zaghete, M. A. and Jaglicic, Z. and Jagodic, M. and Varela, JA",
year = "2015",
abstract = "In this work single phase hexagonal YMnO3 powders were prepared starting from Y(CH3COO)(3)center dot xH(2)O, Mn(CH3COO)(2)center dot 4H(2)O, KMnO4 and KOH using methods of conventional (280 degrees C for 6 h) or microwave assisted hydrothermal synthesis (200 degrees C for 2 h) followed by calcination at 1200 degrees C for 2 h. According to FESEM analysis the calcined powders consisted of submicronic YMnO3 particles, which were uniform in shape and size. Ceramic samples were obtained by sintering the as-synthesized powders at 1400 degrees C for 2 h. XRD analysis confirmed the presence of the single phase hexagonal YMnO3. SEM analysis showed a dense and homogeneous microstructure with typical inter- and intra-grain cracks. Magnetic measurements indicated ferrimagnetic properties that were explained by non-stoichiometry of the obtained compound and an excess of manganese that was confirmed by ICP analysis.",
publisher = "Elsevier Sci Ltd, Oxford",
journal = "Ceramics International",
title = "Hydrothermally assisted synthesis of YMnO3",
pages = "14298-14293",
number = "10",
volume = "41",
doi = "10.1016/j.ceramint.2015.07.060"
}
Branković, Z., Branković, G., Počuča-Nešić, M., Marinković Stanojević, Z., Žunić, M., Luković Golić, D., Tararam, R., Cilense, M., Zaghete, M. A., Jaglicic, Z., Jagodic, M.,& Varela, J.. (2015). Hydrothermally assisted synthesis of YMnO3. in Ceramics International
Elsevier Sci Ltd, Oxford., 41(10), 14293-14298.
https://doi.org/10.1016/j.ceramint.2015.07.060
Branković Z, Branković G, Počuča-Nešić M, Marinković Stanojević Z, Žunić M, Luković Golić D, Tararam R, Cilense M, Zaghete MA, Jaglicic Z, Jagodic M, Varela J. Hydrothermally assisted synthesis of YMnO3. in Ceramics International. 2015;41(10):14293-14298.
doi:10.1016/j.ceramint.2015.07.060 .
Branković, Zorica, Branković, Goran, Počuča-Nešić, Milica, Marinković Stanojević, Zorica, Žunić, Milan, Luković Golić, Danijela, Tararam, R., Cilense, Mario, Zaghete, M. A., Jaglicic, Z., Jagodic, M., Varela, JA, "Hydrothermally assisted synthesis of YMnO3" in Ceramics International, 41, no. 10 (2015):14293-14298,
https://doi.org/10.1016/j.ceramint.2015.07.060 . .
