Barium strontium titanate was obtained by hydrothermal treatment of barium strontium titanate citric precursor solution, previously prepared by complex polymerization method. The thermally induced phase evolution was followed at various temperatures up to 800 A degrees C using thermogravimetric and differential thermal analysis, X-ray diffraction analysis, and Raman spectroscopy. Microstructural characterization of barium strontium titanate powders was performed by scanning and transmission electron microscopy. The proposed synthesis route has been proven as a better and faster method for barium strontium titanate powder preparation as compared to the conventional complex polymerization route. The method was found efficient for production of low agglomerated, fine, nanosized barium strontium titanate powder with well defined stoichiometry, and sub-micron particle size. The results of structural and microstructural characterization showed the complete crystallization of carbonate-free b...arium strontium titanate powder at 700 A degrees C with an average size of crystallites below 50 nm.
TY - JOUR
AU - Ćirković, Jovana
AU - Vojisavljević, Katarina
AU - Šćepanović, Maja
AU - Recnik, Aleksander
AU - Branković, Goran
AU - Branković, Zorica
AU - Srećković, Tatjana
PY - 2013
UR - http://rimsi.imsi.bg.ac.rs/handle/123456789/710
AB - Barium strontium titanate was obtained by hydrothermal treatment of barium strontium titanate citric precursor solution, previously prepared by complex polymerization method. The thermally induced phase evolution was followed at various temperatures up to 800 A degrees C using thermogravimetric and differential thermal analysis, X-ray diffraction analysis, and Raman spectroscopy. Microstructural characterization of barium strontium titanate powders was performed by scanning and transmission electron microscopy. The proposed synthesis route has been proven as a better and faster method for barium strontium titanate powder preparation as compared to the conventional complex polymerization route. The method was found efficient for production of low agglomerated, fine, nanosized barium strontium titanate powder with well defined stoichiometry, and sub-micron particle size. The results of structural and microstructural characterization showed the complete crystallization of carbonate-free barium strontium titanate powder at 700 A degrees C with an average size of crystallites below 50 nm.
PB - Springer, Dordrecht
T2 - Journal of Sol-Gel Science and Technology
T1 - Hydrothermally assisted complex polymerization method for barium strontium titanate powder synthesis
EP - 129
IS - 2
SP - 121
VL - 65
DO - 10.1007/s10971-012-2915-3
ER -
@article{
author = "Ćirković, Jovana and Vojisavljević, Katarina and Šćepanović, Maja and Recnik, Aleksander and Branković, Goran and Branković, Zorica and Srećković, Tatjana",
year = "2013",
abstract = "Barium strontium titanate was obtained by hydrothermal treatment of barium strontium titanate citric precursor solution, previously prepared by complex polymerization method. The thermally induced phase evolution was followed at various temperatures up to 800 A degrees C using thermogravimetric and differential thermal analysis, X-ray diffraction analysis, and Raman spectroscopy. Microstructural characterization of barium strontium titanate powders was performed by scanning and transmission electron microscopy. The proposed synthesis route has been proven as a better and faster method for barium strontium titanate powder preparation as compared to the conventional complex polymerization route. The method was found efficient for production of low agglomerated, fine, nanosized barium strontium titanate powder with well defined stoichiometry, and sub-micron particle size. The results of structural and microstructural characterization showed the complete crystallization of carbonate-free barium strontium titanate powder at 700 A degrees C with an average size of crystallites below 50 nm.",
publisher = "Springer, Dordrecht",
journal = "Journal of Sol-Gel Science and Technology",
title = "Hydrothermally assisted complex polymerization method for barium strontium titanate powder synthesis",
pages = "129-121",
number = "2",
volume = "65",
doi = "10.1007/s10971-012-2915-3"
}
Ćirković, J., Vojisavljević, K., Šćepanović, M., Recnik, A., Branković, G., Branković, Z.,& Srećković, T.. (2013). Hydrothermally assisted complex polymerization method for barium strontium titanate powder synthesis. in Journal of Sol-Gel Science and Technology
Springer, Dordrecht., 65(2), 121-129.
https://doi.org/10.1007/s10971-012-2915-3
Ćirković J, Vojisavljević K, Šćepanović M, Recnik A, Branković G, Branković Z, Srećković T. Hydrothermally assisted complex polymerization method for barium strontium titanate powder synthesis. in Journal of Sol-Gel Science and Technology. 2013;65(2):121-129.
doi:10.1007/s10971-012-2915-3 .
Ćirković, Jovana, Vojisavljević, Katarina, Šćepanović, Maja, Recnik, Aleksander, Branković, Goran, Branković, Zorica, Srećković, Tatjana, "Hydrothermally assisted complex polymerization method for barium strontium titanate powder synthesis" in Journal of Sol-Gel Science and Technology, 65, no. 2 (2013):121-129,
https://doi.org/10.1007/s10971-012-2915-3 . .
