Influence of the type of electrolyte on the morphological and crystallographic characteristics of lead powder particles
2013
Autori
Nikolic, Nebojša DMaksimović, Vesna M
Branković, Goran
Živković, Predrag M.
Pavlović, Miomir G.
Članak u časopisu (Objavljena verzija)
Metapodaci
Prikaz svih podataka o dokumentuApstrakt
Lead electrodeposition processes from basic (nitrate) and complex (acetate) electrolytes were mutually compared by scanning electron microscopy and X-ray diffraction investigation of the produced powder particles. The shape of dendritic particles strongly depended on the type of electrolyte. Dendrites composed of a stalk and weakly developed primary branches (the primary type) were predominantly formed from the basic electrolyte. Ramified dendrites composed of a stalk and of both primary and secondary branches (the secondary type) were mainly formed from the complex electrolyte. In both types of powder particles, Pb crystallites were predominantly oriented in the (111) plane. The formation of powder particles of different shapes with strong (111) preferred orientation is discussed and explained by consideration of the general characteristics of the growth of crystals in electrocrystallization processes.
Ključne reči:
X-ray diffraction (XRD) analysis / scanning electron microscopy (SEM) / powder / lead / electrodeposition / dendriteIzvor:
Journal of the Serbian Chemical Society, 2013, 78, 9, 1387-1395Izdavač:
- Srpsko hemijsko društvo, Beograd
Finansiranje / projekti:
- Elektrohemijska sinteza i karakterizacija nanostrukturiranih funkcionalnih materijala za primenu u novim tehnologijama (RS-MESTD-Basic Research (BR or ON)-172046)
DOI: 10.2298/JSC130211034N
ISSN: 0352-5139
WoS: 000326199200010
Scopus: 2-s2.0-84885139059
Institucija/grupa
Institut za multidisciplinarna istraživanjaTY - JOUR AU - Nikolic, Nebojša D AU - Maksimović, Vesna M AU - Branković, Goran AU - Živković, Predrag M. AU - Pavlović, Miomir G. PY - 2013 UR - http://rimsi.imsi.bg.ac.rs/handle/123456789/693 AB - Lead electrodeposition processes from basic (nitrate) and complex (acetate) electrolytes were mutually compared by scanning electron microscopy and X-ray diffraction investigation of the produced powder particles. The shape of dendritic particles strongly depended on the type of electrolyte. Dendrites composed of a stalk and weakly developed primary branches (the primary type) were predominantly formed from the basic electrolyte. Ramified dendrites composed of a stalk and of both primary and secondary branches (the secondary type) were mainly formed from the complex electrolyte. In both types of powder particles, Pb crystallites were predominantly oriented in the (111) plane. The formation of powder particles of different shapes with strong (111) preferred orientation is discussed and explained by consideration of the general characteristics of the growth of crystals in electrocrystallization processes. PB - Srpsko hemijsko društvo, Beograd T2 - Journal of the Serbian Chemical Society T1 - Influence of the type of electrolyte on the morphological and crystallographic characteristics of lead powder particles EP - 1395 IS - 9 SP - 1387 VL - 78 DO - 10.2298/JSC130211034N ER -
@article{ author = "Nikolic, Nebojša D and Maksimović, Vesna M and Branković, Goran and Živković, Predrag M. and Pavlović, Miomir G.", year = "2013", abstract = "Lead electrodeposition processes from basic (nitrate) and complex (acetate) electrolytes were mutually compared by scanning electron microscopy and X-ray diffraction investigation of the produced powder particles. The shape of dendritic particles strongly depended on the type of electrolyte. Dendrites composed of a stalk and weakly developed primary branches (the primary type) were predominantly formed from the basic electrolyte. Ramified dendrites composed of a stalk and of both primary and secondary branches (the secondary type) were mainly formed from the complex electrolyte. In both types of powder particles, Pb crystallites were predominantly oriented in the (111) plane. The formation of powder particles of different shapes with strong (111) preferred orientation is discussed and explained by consideration of the general characteristics of the growth of crystals in electrocrystallization processes.", publisher = "Srpsko hemijsko društvo, Beograd", journal = "Journal of the Serbian Chemical Society", title = "Influence of the type of electrolyte on the morphological and crystallographic characteristics of lead powder particles", pages = "1395-1387", number = "9", volume = "78", doi = "10.2298/JSC130211034N" }
Nikolic, N. D., Maksimović, V. M., Branković, G., Živković, P. M.,& Pavlović, M. G.. (2013). Influence of the type of electrolyte on the morphological and crystallographic characteristics of lead powder particles. in Journal of the Serbian Chemical Society Srpsko hemijsko društvo, Beograd., 78(9), 1387-1395. https://doi.org/10.2298/JSC130211034N
Nikolic ND, Maksimović VM, Branković G, Živković PM, Pavlović MG. Influence of the type of electrolyte on the morphological and crystallographic characteristics of lead powder particles. in Journal of the Serbian Chemical Society. 2013;78(9):1387-1395. doi:10.2298/JSC130211034N .
Nikolic, Nebojša D, Maksimović, Vesna M, Branković, Goran, Živković, Predrag M., Pavlović, Miomir G., "Influence of the type of electrolyte on the morphological and crystallographic characteristics of lead powder particles" in Journal of the Serbian Chemical Society, 78, no. 9 (2013):1387-1395, https://doi.org/10.2298/JSC130211034N . .