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dc.creatorPantic, Jelena R
dc.creatorKremenović, Aleksandar S
dc.creatorDosen, Anja M
dc.creatorPrekajski, Marija
dc.creatorStanković, Nadezda G
dc.creatorBaščarević, Zvezdana
dc.creatorMatović, Branko
dc.date.accessioned2022-04-05T14:44:15Z
dc.date.available2022-04-05T14:44:15Z
dc.date.issued2013
dc.identifier.issn0272-8842
dc.identifier.urihttp://rimsi.imsi.bg.ac.rs/handle/123456789/689
dc.description.abstractSphene (CaTiSiO5), a calcium titanosilicate ceramic has been prepared from a powder mixture of CaCO3, TiO2 and SiO2 using vibromilling for homogenization and activation of precursors. The mechanochemical process initially yielded amorphous powders, which on further calcination, crystallized to yield sphene ceramic. The evolution of the phase composition with thermal treatment was investigated by X-ray powder diffraction (XRPD). Powder morphology and particle size distribution were analyzed by scanning electron microscopy (SEM) and laser diffraction, respectively. Rietveld refinement was employed to get the structural information of the synthesized powder. Densification and microstructure evolution was determined by means of density and scanning electron microscopy (SEM). The most favorable conditions for mechanical activation and synthesis of sphene based ceramic material are reported.en
dc.publisherElsevier Sci Ltd, Oxford
dc.relationinfo:eu-repo/grantAgreement/MESTD/Integrated and Interdisciplinary Research (IIR or III)/45012/RS//
dc.relationinfo:eu-repo/grantAgreement/MESTD/Basic Research (BR or ON)/176016/RS//
dc.rightsrestrictedAccess
dc.sourceCeramics International
dc.subjectSpheneen
dc.subjectSEM/EDSen
dc.subjectRietveld refinementen
dc.subjectMechanochemistryen
dc.titleInfluence of mechanical activation on sphene based ceramic material synthesisen
dc.typearticle
dc.rights.licenseARR
dc.citation.epage488
dc.citation.issue1
dc.citation.other39(1): 483-488
dc.citation.rankM21
dc.citation.spage483
dc.citation.volume39
dc.identifier.doi10.1016/j.ceramint.2012.06.052
dc.identifier.scopus2-s2.0-84869092286
dc.identifier.wos000315246300063
dc.type.versionpublishedVersion


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Приказ основних података о документу