Influence of mechanical activation on sphene based ceramic material synthesis
Samo za registrovane korisnike
2013
Autori
Pantic, Jelena RKremenović, Aleksandar S
Dosen, Anja M
Prekajski, Marija
Stanković, Nadezda G
Baščarević, Zvezdana
Matović, Branko
Članak u časopisu (Objavljena verzija)
Metapodaci
Prikaz svih podataka o dokumentuApstrakt
Sphene (CaTiSiO5), a calcium titanosilicate ceramic has been prepared from a powder mixture of CaCO3, TiO2 and SiO2 using vibromilling for homogenization and activation of precursors. The mechanochemical process initially yielded amorphous powders, which on further calcination, crystallized to yield sphene ceramic. The evolution of the phase composition with thermal treatment was investigated by X-ray powder diffraction (XRPD). Powder morphology and particle size distribution were analyzed by scanning electron microscopy (SEM) and laser diffraction, respectively. Rietveld refinement was employed to get the structural information of the synthesized powder. Densification and microstructure evolution was determined by means of density and scanning electron microscopy (SEM). The most favorable conditions for mechanical activation and synthesis of sphene based ceramic material are reported.
Ključne reči:
Sphene / SEM/EDS / Rietveld refinement / MechanochemistryIzvor:
Ceramics International, 2013, 39, 1, 483-488Izdavač:
- Elsevier Sci Ltd, Oxford
Finansiranje / projekti:
- Sinteza, procesiranje i karakterizacija nanostrukturnih materijala za primenu u oblasti energije, mehaničkog inženjerstva, zaštite životne stredine i biomedicine (RS-MESTD-Integrated and Interdisciplinary Research (IIR or III)-45012)
- Magmatizam i geodinamika Balkanskog poluostrva od mezozoika do danas: značaj za obrazovanje metaličnih i nemetaličnih rudnih ležišta (RS-MESTD-Basic Research (BR or ON)-176016)
DOI: 10.1016/j.ceramint.2012.06.052
ISSN: 0272-8842
WoS: 000315246300063
Scopus: 2-s2.0-84869092286
Institucija/grupa
Institut za multidisciplinarna istraživanjaTY - JOUR AU - Pantic, Jelena R AU - Kremenović, Aleksandar S AU - Dosen, Anja M AU - Prekajski, Marija AU - Stanković, Nadezda G AU - Baščarević, Zvezdana AU - Matović, Branko PY - 2013 UR - http://rimsi.imsi.bg.ac.rs/handle/123456789/689 AB - Sphene (CaTiSiO5), a calcium titanosilicate ceramic has been prepared from a powder mixture of CaCO3, TiO2 and SiO2 using vibromilling for homogenization and activation of precursors. The mechanochemical process initially yielded amorphous powders, which on further calcination, crystallized to yield sphene ceramic. The evolution of the phase composition with thermal treatment was investigated by X-ray powder diffraction (XRPD). Powder morphology and particle size distribution were analyzed by scanning electron microscopy (SEM) and laser diffraction, respectively. Rietveld refinement was employed to get the structural information of the synthesized powder. Densification and microstructure evolution was determined by means of density and scanning electron microscopy (SEM). The most favorable conditions for mechanical activation and synthesis of sphene based ceramic material are reported. PB - Elsevier Sci Ltd, Oxford T2 - Ceramics International T1 - Influence of mechanical activation on sphene based ceramic material synthesis EP - 488 IS - 1 SP - 483 VL - 39 DO - 10.1016/j.ceramint.2012.06.052 ER -
@article{ author = "Pantic, Jelena R and Kremenović, Aleksandar S and Dosen, Anja M and Prekajski, Marija and Stanković, Nadezda G and Baščarević, Zvezdana and Matović, Branko", year = "2013", abstract = "Sphene (CaTiSiO5), a calcium titanosilicate ceramic has been prepared from a powder mixture of CaCO3, TiO2 and SiO2 using vibromilling for homogenization and activation of precursors. The mechanochemical process initially yielded amorphous powders, which on further calcination, crystallized to yield sphene ceramic. The evolution of the phase composition with thermal treatment was investigated by X-ray powder diffraction (XRPD). Powder morphology and particle size distribution were analyzed by scanning electron microscopy (SEM) and laser diffraction, respectively. Rietveld refinement was employed to get the structural information of the synthesized powder. Densification and microstructure evolution was determined by means of density and scanning electron microscopy (SEM). The most favorable conditions for mechanical activation and synthesis of sphene based ceramic material are reported.", publisher = "Elsevier Sci Ltd, Oxford", journal = "Ceramics International", title = "Influence of mechanical activation on sphene based ceramic material synthesis", pages = "488-483", number = "1", volume = "39", doi = "10.1016/j.ceramint.2012.06.052" }
Pantic, J. R., Kremenović, A. S., Dosen, A. M., Prekajski, M., Stanković, N. G., Baščarević, Z.,& Matović, B.. (2013). Influence of mechanical activation on sphene based ceramic material synthesis. in Ceramics International Elsevier Sci Ltd, Oxford., 39(1), 483-488. https://doi.org/10.1016/j.ceramint.2012.06.052
Pantic JR, Kremenović AS, Dosen AM, Prekajski M, Stanković NG, Baščarević Z, Matović B. Influence of mechanical activation on sphene based ceramic material synthesis. in Ceramics International. 2013;39(1):483-488. doi:10.1016/j.ceramint.2012.06.052 .
Pantic, Jelena R, Kremenović, Aleksandar S, Dosen, Anja M, Prekajski, Marija, Stanković, Nadezda G, Baščarević, Zvezdana, Matović, Branko, "Influence of mechanical activation on sphene based ceramic material synthesis" in Ceramics International, 39, no. 1 (2013):483-488, https://doi.org/10.1016/j.ceramint.2012.06.052 . .