ZnTiO3 Ceramic Nanopowder Microstructure Changes During Compaction

2013
Authors
Labus, Nebojša J.
Krstic, Jelena D

Marković, Smilja

Vasiljević-Radović, Dana

Nikolić, Maria Vesna

Pavlović, Vera P.

Article (Published version)
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ZnTiO3 nanopowder as a constitutive component in compact production was primarily characterised. Scanning electron micrographs of as received powder were recorded. Mercury porosimetry and nitrogen adsorption were also performed on loose powder. Particle size distribution in a water powder suspension was determined with a laser particle size analyser. Compaction was performed on different pressures in a range from 100 to 400 MPa using the uniaxial double sided compaction technique without binder and lubricant. Micrographs of compacted specimens were obtained using scanning electron microscopy and atomic force microscopy. Pore size distribution was also determined by mercury porosimetry and nitrogen adsorption. Results revealed that with increasing pressure during compaction interagglomerate pores diminish in size until they reach some critical diameter related to the intra-agglomerate pore size.
Keywords:
Pore size distribution / Nitrogen adsorption / Nanopowder / Mercury porosimetry / CompactionSource:
Science of Sintering, 2013, 45, 2, 209-221Publisher:
- Međunarodni Institut za nauku o sinterovanju, Beograd
DOI: 10.2298/SOS1302209L
ISSN: 0350-820X
WoS: 000323550700010
Scopus: 2-s2.0-84881537663
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Institut za multidisciplinarna istraživanjaTY - JOUR AU - Labus, Nebojša J. AU - Krstic, Jelena D AU - Marković, Smilja AU - Vasiljević-Radović, Dana AU - Nikolić, Maria Vesna AU - Pavlović, Vera P. PY - 2013 UR - http://rimsi.imsi.bg.ac.rs/handle/123456789/667 AB - ZnTiO3 nanopowder as a constitutive component in compact production was primarily characterised. Scanning electron micrographs of as received powder were recorded. Mercury porosimetry and nitrogen adsorption were also performed on loose powder. Particle size distribution in a water powder suspension was determined with a laser particle size analyser. Compaction was performed on different pressures in a range from 100 to 400 MPa using the uniaxial double sided compaction technique without binder and lubricant. Micrographs of compacted specimens were obtained using scanning electron microscopy and atomic force microscopy. Pore size distribution was also determined by mercury porosimetry and nitrogen adsorption. Results revealed that with increasing pressure during compaction interagglomerate pores diminish in size until they reach some critical diameter related to the intra-agglomerate pore size. PB - Međunarodni Institut za nauku o sinterovanju, Beograd T2 - Science of Sintering T1 - ZnTiO3 Ceramic Nanopowder Microstructure Changes During Compaction EP - 221 IS - 2 SP - 209 VL - 45 DO - 10.2298/SOS1302209L ER -
@article{ author = "Labus, Nebojša J. and Krstic, Jelena D and Marković, Smilja and Vasiljević-Radović, Dana and Nikolić, Maria Vesna and Pavlović, Vera P.", year = "2013", abstract = "ZnTiO3 nanopowder as a constitutive component in compact production was primarily characterised. Scanning electron micrographs of as received powder were recorded. Mercury porosimetry and nitrogen adsorption were also performed on loose powder. Particle size distribution in a water powder suspension was determined with a laser particle size analyser. Compaction was performed on different pressures in a range from 100 to 400 MPa using the uniaxial double sided compaction technique without binder and lubricant. Micrographs of compacted specimens were obtained using scanning electron microscopy and atomic force microscopy. Pore size distribution was also determined by mercury porosimetry and nitrogen adsorption. Results revealed that with increasing pressure during compaction interagglomerate pores diminish in size until they reach some critical diameter related to the intra-agglomerate pore size.", publisher = "Međunarodni Institut za nauku o sinterovanju, Beograd", journal = "Science of Sintering", title = "ZnTiO3 Ceramic Nanopowder Microstructure Changes During Compaction", pages = "221-209", number = "2", volume = "45", doi = "10.2298/SOS1302209L" }
Labus, N. J., Krstic, J. D., Marković, S., Vasiljević-Radović, D., Nikolić, M. V.,& Pavlović, V. P.. (2013). ZnTiO3 Ceramic Nanopowder Microstructure Changes During Compaction. in Science of Sintering Međunarodni Institut za nauku o sinterovanju, Beograd., 45(2), 209-221. https://doi.org/10.2298/SOS1302209L
Labus NJ, Krstic JD, Marković S, Vasiljević-Radović D, Nikolić MV, Pavlović VP. ZnTiO3 Ceramic Nanopowder Microstructure Changes During Compaction. in Science of Sintering. 2013;45(2):209-221. doi:10.2298/SOS1302209L .
Labus, Nebojša J., Krstic, Jelena D, Marković, Smilja, Vasiljević-Radović, Dana, Nikolić, Maria Vesna, Pavlović, Vera P., "ZnTiO3 Ceramic Nanopowder Microstructure Changes During Compaction" in Science of Sintering, 45, no. 2 (2013):209-221, https://doi.org/10.2298/SOS1302209L . .