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ZnTiO3 Ceramic Nanopowder Microstructure Changes During Compaction

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2013
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Authors
Labus, Nebojša J.
Krstic, Jelena D
Marković, Smilja
Vasiljević-Radović, Dana
Nikolić, Maria Vesna
Pavlović, Vera P.
Article (Published version)
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Abstract
ZnTiO3 nanopowder as a constitutive component in compact production was primarily characterised. Scanning electron micrographs of as received powder were recorded. Mercury porosimetry and nitrogen adsorption were also performed on loose powder. Particle size distribution in a water powder suspension was determined with a laser particle size analyser. Compaction was performed on different pressures in a range from 100 to 400 MPa using the uniaxial double sided compaction technique without binder and lubricant. Micrographs of compacted specimens were obtained using scanning electron microscopy and atomic force microscopy. Pore size distribution was also determined by mercury porosimetry and nitrogen adsorption. Results revealed that with increasing pressure during compaction interagglomerate pores diminish in size until they reach some critical diameter related to the intra-agglomerate pore size.
Keywords:
Pore size distribution / Nitrogen adsorption / Nanopowder / Mercury porosimetry / Compaction
Source:
Science of Sintering, 2013, 45, 2, 209-221
Publisher:
  • Međunarodni Institut za nauku o sinterovanju, Beograd

DOI: 10.2298/SOS1302209L

ISSN: 0350-820X

WoS: 000323550700010

Scopus: 2-s2.0-84881537663
[ Google Scholar ]
4
4
URI
http://rimsi.imsi.bg.ac.rs/handle/123456789/667
Collections
  • Radovi istraživača / Researchers’ publications
Institution/Community
Institut za multidisciplinarna istraživanja
TY  - JOUR
AU  - Labus, Nebojša J.
AU  - Krstic, Jelena D
AU  - Marković, Smilja
AU  - Vasiljević-Radović, Dana
AU  - Nikolić, Maria Vesna
AU  - Pavlović, Vera P.
PY  - 2013
UR  - http://rimsi.imsi.bg.ac.rs/handle/123456789/667
AB  - ZnTiO3 nanopowder as a constitutive component in compact production was primarily characterised. Scanning electron micrographs of as received powder were recorded. Mercury porosimetry and nitrogen adsorption were also performed on loose powder. Particle size distribution in a water powder suspension was determined with a laser particle size analyser. Compaction was performed on different pressures in a range from 100 to 400 MPa using the uniaxial double sided compaction technique without binder and lubricant. Micrographs of compacted specimens were obtained using scanning electron microscopy and atomic force microscopy. Pore size distribution was also determined by mercury porosimetry and nitrogen adsorption. Results revealed that with increasing pressure during compaction interagglomerate pores diminish in size until they reach some critical diameter related to the intra-agglomerate pore size.
PB  - Međunarodni Institut za nauku o sinterovanju, Beograd
T2  - Science of Sintering
T1  - ZnTiO3 Ceramic Nanopowder Microstructure Changes During Compaction
EP  - 221
IS  - 2
SP  - 209
VL  - 45
DO  - 10.2298/SOS1302209L
ER  - 
@article{
author = "Labus, Nebojša J. and Krstic, Jelena D and Marković, Smilja and Vasiljević-Radović, Dana and Nikolić, Maria Vesna and Pavlović, Vera P.",
year = "2013",
abstract = "ZnTiO3 nanopowder as a constitutive component in compact production was primarily characterised. Scanning electron micrographs of as received powder were recorded. Mercury porosimetry and nitrogen adsorption were also performed on loose powder. Particle size distribution in a water powder suspension was determined with a laser particle size analyser. Compaction was performed on different pressures in a range from 100 to 400 MPa using the uniaxial double sided compaction technique without binder and lubricant. Micrographs of compacted specimens were obtained using scanning electron microscopy and atomic force microscopy. Pore size distribution was also determined by mercury porosimetry and nitrogen adsorption. Results revealed that with increasing pressure during compaction interagglomerate pores diminish in size until they reach some critical diameter related to the intra-agglomerate pore size.",
publisher = "Međunarodni Institut za nauku o sinterovanju, Beograd",
journal = "Science of Sintering",
title = "ZnTiO3 Ceramic Nanopowder Microstructure Changes During Compaction",
pages = "221-209",
number = "2",
volume = "45",
doi = "10.2298/SOS1302209L"
}
Labus, N. J., Krstic, J. D., Marković, S., Vasiljević-Radović, D., Nikolić, M. V.,& Pavlović, V. P.. (2013). ZnTiO3 Ceramic Nanopowder Microstructure Changes During Compaction. in Science of Sintering
Međunarodni Institut za nauku o sinterovanju, Beograd., 45(2), 209-221.
https://doi.org/10.2298/SOS1302209L
Labus NJ, Krstic JD, Marković S, Vasiljević-Radović D, Nikolić MV, Pavlović VP. ZnTiO3 Ceramic Nanopowder Microstructure Changes During Compaction. in Science of Sintering. 2013;45(2):209-221.
doi:10.2298/SOS1302209L .
Labus, Nebojša J., Krstic, Jelena D, Marković, Smilja, Vasiljević-Radović, Dana, Nikolić, Maria Vesna, Pavlović, Vera P., "ZnTiO3 Ceramic Nanopowder Microstructure Changes During Compaction" in Science of Sintering, 45, no. 2 (2013):209-221,
https://doi.org/10.2298/SOS1302209L . .

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