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dc.creatorLuković Golić, Danijela
dc.creatorBranković, Zorica
dc.creatorDaneu, Nina
dc.creatorBernik, Slavko
dc.creatorBranković, Goran
dc.date.accessioned2022-04-05T14:35:56Z
dc.date.available2022-04-05T14:35:56Z
dc.date.issued2012
dc.identifier.issn0928-0707
dc.identifier.urihttp://rimsi.imsi.bg.ac.rs/handle/123456789/562
dc.description.abstractZinc oxide powders with different morphologies and grain sizes were synthesized using solvothermal methods from ethanolic zinc acetate solutions in the presence of lithium hydroxide. The influence of the temperature and the time of the reaction, as well as the pH value of the starting solution, on the ZnO particle size and morphology were examined. It was found that an increase in the pH value from 8 to 12 results in a significant decrease in the mean particle size. Also, the particles' morphology can be changed from hexagonal plates and prisms to rods by controlling the reaction time and the temperature. The crystallization mechanism is discussed, based on established correlations such as the particle size/shape versus the reaction parameters. Dissolution/recrystallisation is the most probable growth mechanism responsible for the ZnO particles' morphology obtained in the solvothermal (hydrothermal) reactions with a basic solution. The planar structure of the zinc-hydroxy-acetate molecule plays the main role in growing the structures during the sovothermal reactions with a slightly acid solution.en
dc.publisherSpringer, Dordrecht
dc.relationinfo:eu-repo/grantAgreement/MESTD/Integrated and Interdisciplinary Research (IIR or III)/45007/RS//
dc.relationSlovenian Research AgencySlovenian Research Agency - Slovenia [P2-0084-0106, L2-4192]
dc.rightsrestrictedAccess
dc.sourceJournal of Sol-Gel Science and Technology
dc.subjectZnOen
dc.subjectSolvothermal synthesisen
dc.subjectSol-gelen
dc.subjectReaction parametersen
dc.subjectParticle morphologyen
dc.titleSolvothermal syntheses of nano- and micro-sized ZnO powders with a controllable morphologyen
dc.typearticle
dc.rights.licenseARR
dc.citation.epage125
dc.citation.issue1
dc.citation.other63(1): 116-125
dc.citation.rankM21
dc.citation.spage116
dc.citation.volume63
dc.identifier.doi10.1007/s10971-012-2773-z
dc.identifier.scopus2-s2.0-84863318558
dc.identifier.wos000305684000015
dc.type.versionpublishedVersion


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