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Structural characterization of self-assembled ZnO nanoparticles obtained by the sol-gel method from Zn(CH3COO)(2)center dot 2H(2)O

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Authors
Luković Golić, Danijela
Branković, Goran
Počuča-Nešić, Milica
Vojisavljević, Katarina
Recnik, Aleksander
Daneu, Nina
Bernik, Slavko
Šćepanović, Maja
Poleti, Dejan
Branković, Zorica
Article (Published version)
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Abstract
Zinc oxide nanopowders were synthesized by the sol-gel method from an ethanol solution of zinc acetate dihydrate. Detailed structural and microstructural investigations were carried out using x-ray diffraction, Raman spectroscopy, thermogravimetric and differential thermal analyses, as well as high-resolution transmission electron microscopy (TEM) and field-emission scanning electron microscopy. The intermediate compound of the reaction was layered zinc hydroxide acetate that further transforms into hexagonally shaped ZnO crystalline nanoplates (d(m) = 4 nm), which aggregate into larger spherical particles. According to the TEM analysis the ZnO nanoparticles were self-assembled into larger particles with the same orientation, i.e. aligned lattice planes of the particles. A further solvothermal treatment resulted in hexagonal, prismatic ZnO mesocrystals.
Source:
Nanotechnology, 2011, 22, 39
Publisher:
  • IOP Publishing Ltd, Bristol
Funding / projects:
  • Zero- to Three-Dimensional Nanostructures for Application in Electronics and Renewable Energy Sources: Synthesis, Characterization and Processing (RS-45007)
  • Slovenian Research AgencySlovenian Research Agency - Slovenia [P2-0084-0106]

DOI: 10.1088/0957-4484/22/39/395603

ISSN: 0957-4484

PubMed: 21891855

WoS: 000294723700016

Scopus: 2-s2.0-80052538080
[ Google Scholar ]
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33
URI
http://rimsi.imsi.bg.ac.rs/handle/123456789/469
Collections
  • Radovi istraživača / Researchers’ publications
Institution/Community
Institut za multidisciplinarna istraživanja
TY  - JOUR
AU  - Luković Golić, Danijela
AU  - Branković, Goran
AU  - Počuča-Nešić, Milica
AU  - Vojisavljević, Katarina
AU  - Recnik, Aleksander
AU  - Daneu, Nina
AU  - Bernik, Slavko
AU  - Šćepanović, Maja
AU  - Poleti, Dejan
AU  - Branković, Zorica
PY  - 2011
UR  - http://rimsi.imsi.bg.ac.rs/handle/123456789/469
AB  - Zinc oxide nanopowders were synthesized by the sol-gel method from an ethanol solution of zinc acetate dihydrate. Detailed structural and microstructural investigations were carried out using x-ray diffraction, Raman spectroscopy, thermogravimetric and differential thermal analyses, as well as high-resolution transmission electron microscopy (TEM) and field-emission scanning electron microscopy. The intermediate compound of the reaction was layered zinc hydroxide acetate that further transforms into hexagonally shaped ZnO crystalline nanoplates (d(m) = 4 nm), which aggregate into larger spherical particles. According to the TEM analysis the ZnO nanoparticles were self-assembled into larger particles with the same orientation, i.e. aligned lattice planes of the particles. A further solvothermal treatment resulted in hexagonal, prismatic ZnO mesocrystals.
PB  - IOP Publishing Ltd, Bristol
T2  - Nanotechnology
T1  - Structural characterization of self-assembled ZnO nanoparticles obtained by the sol-gel method from Zn(CH3COO)(2)center dot 2H(2)O
IS  - 39
VL  - 22
DO  - 10.1088/0957-4484/22/39/395603
ER  - 
@article{
author = "Luković Golić, Danijela and Branković, Goran and Počuča-Nešić, Milica and Vojisavljević, Katarina and Recnik, Aleksander and Daneu, Nina and Bernik, Slavko and Šćepanović, Maja and Poleti, Dejan and Branković, Zorica",
year = "2011",
abstract = "Zinc oxide nanopowders were synthesized by the sol-gel method from an ethanol solution of zinc acetate dihydrate. Detailed structural and microstructural investigations were carried out using x-ray diffraction, Raman spectroscopy, thermogravimetric and differential thermal analyses, as well as high-resolution transmission electron microscopy (TEM) and field-emission scanning electron microscopy. The intermediate compound of the reaction was layered zinc hydroxide acetate that further transforms into hexagonally shaped ZnO crystalline nanoplates (d(m) = 4 nm), which aggregate into larger spherical particles. According to the TEM analysis the ZnO nanoparticles were self-assembled into larger particles with the same orientation, i.e. aligned lattice planes of the particles. A further solvothermal treatment resulted in hexagonal, prismatic ZnO mesocrystals.",
publisher = "IOP Publishing Ltd, Bristol",
journal = "Nanotechnology",
title = "Structural characterization of self-assembled ZnO nanoparticles obtained by the sol-gel method from Zn(CH3COO)(2)center dot 2H(2)O",
number = "39",
volume = "22",
doi = "10.1088/0957-4484/22/39/395603"
}
Luković Golić, D., Branković, G., Počuča-Nešić, M., Vojisavljević, K., Recnik, A., Daneu, N., Bernik, S., Šćepanović, M., Poleti, D.,& Branković, Z.. (2011). Structural characterization of self-assembled ZnO nanoparticles obtained by the sol-gel method from Zn(CH3COO)(2)center dot 2H(2)O. in Nanotechnology
IOP Publishing Ltd, Bristol., 22(39).
https://doi.org/10.1088/0957-4484/22/39/395603
Luković Golić D, Branković G, Počuča-Nešić M, Vojisavljević K, Recnik A, Daneu N, Bernik S, Šćepanović M, Poleti D, Branković Z. Structural characterization of self-assembled ZnO nanoparticles obtained by the sol-gel method from Zn(CH3COO)(2)center dot 2H(2)O. in Nanotechnology. 2011;22(39).
doi:10.1088/0957-4484/22/39/395603 .
Luković Golić, Danijela, Branković, Goran, Počuča-Nešić, Milica, Vojisavljević, Katarina, Recnik, Aleksander, Daneu, Nina, Bernik, Slavko, Šćepanović, Maja, Poleti, Dejan, Branković, Zorica, "Structural characterization of self-assembled ZnO nanoparticles obtained by the sol-gel method from Zn(CH3COO)(2)center dot 2H(2)O" in Nanotechnology, 22, no. 39 (2011),
https://doi.org/10.1088/0957-4484/22/39/395603 . .

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