Properties of lanthanum doped BaTiO3 produced from nanopowders
Abstract
Pure and barium titanate (BT) powders doped with different lanthanum concentration were prepared by the polymeric precursor method (Pechini process) which was carried out as a three-stage process from organometallic complexes. Sintering of pressed powders was performed at 1300 degrees C for 2, 4 and 8 h. XRD analysis showed cubic BT powders with crystallite sizes between 20 and 25 nm and tetragonal crystal structure of BT ceramics. The influence of sintering time on grain growth was fairly obvious. It was found that lanthanum doping has significant effect on powders particle size and ceramics grain size. The influence of lanthanum concentration on grain size inhibition, improving the dielectric properties of BT ceramics was detected. The relation between sintering time, grain size, structure and electrical properties of the BT ceramics was analyzed.
Keywords:
Precursors: organic / Microstructure / Dielectric properties / BaTiO3Source:
Ceramics International, 2010, 36, 6, 1817-1824Publisher:
- Elsevier Sci Ltd, Oxford
Funding / projects:
- COST 539
- Sinteza nanoprahova i dobijanje keramike i nanokompozita za primenu u novim tehnologijama (RS-142059)
- Synthesis, characterization and activity of organic and coordination composition and their application in (bio) nanotechnology (RS-142010)
DOI: 10.1016/j.ceramint.2010.03.010
ISSN: 0272-8842
WoS: 000280027800009
Scopus: 2-s2.0-77953959053
Collections
Institution/Community
Institut za multidisciplinarna istraživanjaTY - JOUR AU - Vijatović-Petrović, Mirjana AU - Stojanović, Biljana D AU - Bobić, Jelena AU - Ramoska, T AU - Bowen, P PY - 2010 UR - http://rimsi.imsi.bg.ac.rs/handle/123456789/428 AB - Pure and barium titanate (BT) powders doped with different lanthanum concentration were prepared by the polymeric precursor method (Pechini process) which was carried out as a three-stage process from organometallic complexes. Sintering of pressed powders was performed at 1300 degrees C for 2, 4 and 8 h. XRD analysis showed cubic BT powders with crystallite sizes between 20 and 25 nm and tetragonal crystal structure of BT ceramics. The influence of sintering time on grain growth was fairly obvious. It was found that lanthanum doping has significant effect on powders particle size and ceramics grain size. The influence of lanthanum concentration on grain size inhibition, improving the dielectric properties of BT ceramics was detected. The relation between sintering time, grain size, structure and electrical properties of the BT ceramics was analyzed. PB - Elsevier Sci Ltd, Oxford T2 - Ceramics International T1 - Properties of lanthanum doped BaTiO3 produced from nanopowders EP - 1824 IS - 6 SP - 1817 VL - 36 DO - 10.1016/j.ceramint.2010.03.010 ER -
@article{ author = "Vijatović-Petrović, Mirjana and Stojanović, Biljana D and Bobić, Jelena and Ramoska, T and Bowen, P", year = "2010", abstract = "Pure and barium titanate (BT) powders doped with different lanthanum concentration were prepared by the polymeric precursor method (Pechini process) which was carried out as a three-stage process from organometallic complexes. Sintering of pressed powders was performed at 1300 degrees C for 2, 4 and 8 h. XRD analysis showed cubic BT powders with crystallite sizes between 20 and 25 nm and tetragonal crystal structure of BT ceramics. The influence of sintering time on grain growth was fairly obvious. It was found that lanthanum doping has significant effect on powders particle size and ceramics grain size. The influence of lanthanum concentration on grain size inhibition, improving the dielectric properties of BT ceramics was detected. The relation between sintering time, grain size, structure and electrical properties of the BT ceramics was analyzed.", publisher = "Elsevier Sci Ltd, Oxford", journal = "Ceramics International", title = "Properties of lanthanum doped BaTiO3 produced from nanopowders", pages = "1824-1817", number = "6", volume = "36", doi = "10.1016/j.ceramint.2010.03.010" }
Vijatović-Petrović, M., Stojanović, B. D., Bobić, J., Ramoska, T.,& Bowen, P.. (2010). Properties of lanthanum doped BaTiO3 produced from nanopowders. in Ceramics International Elsevier Sci Ltd, Oxford., 36(6), 1817-1824. https://doi.org/10.1016/j.ceramint.2010.03.010
Vijatović-Petrović M, Stojanović BD, Bobić J, Ramoska T, Bowen P. Properties of lanthanum doped BaTiO3 produced from nanopowders. in Ceramics International. 2010;36(6):1817-1824. doi:10.1016/j.ceramint.2010.03.010 .
Vijatović-Petrović, Mirjana, Stojanović, Biljana D, Bobić, Jelena, Ramoska, T, Bowen, P, "Properties of lanthanum doped BaTiO3 produced from nanopowders" in Ceramics International, 36, no. 6 (2010):1817-1824, https://doi.org/10.1016/j.ceramint.2010.03.010 . .