Приказ основних података о документу
Morphology of Fe-Ni alloy powders electrodeposited from citrate-sulfate containing solutions
Morfologija prahova Fe-Ni legura elektrohemijski istaloženih iz citratno-sulfatnih rastvora
dc.creator | Lačnjevac, Uroš | |
dc.creator | D. Jović, Vladimir | |
dc.creator | Jović, Borka M | |
dc.creator | Baščarević, Zvezdana | |
dc.creator | Maksimović, Vesna M | |
dc.creator | Pavlović, Miomir | |
dc.date.accessioned | 2023-12-09T13:47:55Z | |
dc.date.available | 2023-12-09T13:47:55Z | |
dc.date.issued | 2011 | |
dc.identifier.issn | 0351-9465 | |
dc.identifier.uri | http://rimsi.imsi.bg.ac.rs/handle/123456789/2975 | |
dc.description.abstract | The electrochemical deposition of the Fe-Ni alloy powders from citrate-sulfate containing electrolytes of different Ni/Fe ions concentration ratios at pH 4.5 was examined by the polarization measurements. All polarization curves have a similar shape and are characterized by the presence of two inflection points. The first inflection point reflects the beginning of alloy deposition, while the second one (˜) corresponds to the moment when the cathode reaction becomes determined by the rate of hydrogen bubbles formation. The potentials of Fe-Ni alloys deposition at all investigated Ni/Fe ratios are more positive than those for pure metal powders deposition. As the Ni/Fe ratio decreases, the polarization curves are placed at slightly more positive potentials. The morphology of electrodeposited powder particles was investigated using scanning electron microscopy (SEM). A common characteristic of all Fe-Ni alloy powders is the presence of cone shaped cavities. Powder particles electrodeposited at the ratio Ni/Fe = 9/1 are mainly consisted of nodules of either very flat surface or rough surface, with well defined crystals detected only on a few particles. With the decrease of the Ni/Fe ratio, the presence of well defined crystals on the nodule surface becomes more pronounced. In the powder with the highest amount of Fe (Ni/Fe = 1/3), the whole surface of all particles is covered with crystals of different shapes. | sr |
dc.description.abstract | Elektrohemijsko taloženje prahova Fe-Ni legura ispitivano je snimanjem polarizacionih dijagrama u citratno-sulfatnim rastvorima pri različitom odnosu koncentracija Ni/Fe jona na pH 4,5. Sve polarizacione krive imaju sličan oblik i okarakterisane su prisustvom dve prevojne tačke na dijagramu. Prva prevojna tačka odgovara početku taloženja Fe-Ni legure, dok druga predstavlja momenat kada ukupna elektrohemijska reakcija postaje kontrolisana brzinom formiranja mehurova vodonika. Potencijali taloženja Fe-Ni legura pri svim ispitivanim odnosima Ni/Fe pozitivniji su od potencijala taloženja čistih metala, pri čemu se sa smanjenjem odnosa Ni/Fe polarizacione krive pomeraju ka malo pozitivnijim vrednostima potencijala. Morfologija čestica prahova ispitivana je korišćenjem skenirajuće elektronske mikroskopije (SEM). Zajednička karakteristika svih prahova Fe-Ni legura je prisustvo šupljina konusnog oblika. Čestice praha istaloženog pri odnosu Ni/Fe = 9/1 uglavnom su sastavljene od čvorića, glatke ili neravne površine, kod kojih se na pojedinim mestima mogu uočiti dobro definisani kristali. Sa smanjenjem odnosa Ni/Fe, prisustvo kristala na površini čvorića postaje sve izraženije, dok su kod praha sa najvećim sadržajem Fe (Ni/Fe = 1/3) na celoj površini čestica prisutni kristali različitog oblika. | sr |
dc.language.iso | sr | sr |
dc.publisher | Belgrade, Serbia : Engineering Society for Corrosion | sr |
dc.rights | openAccess | sr |
dc.rights.uri | https://creativecommons.org/licenses/by/4.0/ | |
dc.source | Zaštita materijala | sr |
dc.subject | morphology | sr |
dc.subject | Fe-Ni alloy powders | sr |
dc.subject | electro-deposition | sr |
dc.subject | SEM | sr |
dc.subject | morfologija | sr |
dc.subject | prahovi legura Fe-Ni | sr |
dc.subject | taloženje | sr |
dc.subject | SEM | sr |
dc.title | Morphology of Fe-Ni alloy powders electrodeposited from citrate-sulfate containing solutions | sr |
dc.title | Morfologija prahova Fe-Ni legura elektrohemijski istaloženih iz citratno-sulfatnih rastvora | sr |
dc.type | article | sr |
dc.rights.license | BY | sr |
dc.citation.epage | 241 | |
dc.citation.issue | 4 | |
dc.citation.rank | M52 | |
dc.citation.spage | 237 | |
dc.citation.volume | 52 | |
dc.identifier.fulltext | http://rimsi.imsi.bg.ac.rs/bitstream/id/7624/ZM_52_4_237.pdf | |
dc.identifier.rcub | https://hdl.handle.net/21.15107/rcub_rimsi_2975 | |
dc.type.version | publishedVersion | sr |