A detailed XRD and FTIR analysis of Bi2O3 doped ZnO-SnO2 ceramics
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Ivetić, Tamara B.Nikolić, Maria Vesna

Paraskevopoulos, K.M.
Blagojević, V.
Nikolić, Pantelija M.

Ristić, M.M.
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ZnO-SnO2 ceramics were prepared with a traditional powder mixed oxide route by mixing starting powders of ZnO and SnO2 in the molar ratio 2:1 and adding small amounts (0.5; 1.0; and 1.5 molar%) of Bi 2O3. These mixtures were then mechanically activated for 10 minutes in a planetary ball mill, uniaxially pressed and sintered at 1300°C for 2h. The phase composition of the sintered samples was determined with X-ray Diffraction (XRD) analysis and a detailed Rietveld analysis was performed. Room temperature far infrared reflectivity diagrams were obtained using Bruker 113V FTIR spectrometer and fitted with several theoretical models in other to determine parameter values for some structural and optical properties of the obtained material.
Keywords:
Structu / Starting powders / Sintered samples / Room temperature / Planetary ball mill / Parameter values / Molar ratio / Mixed oxide route / FT-IR-spectrometers / FTIR analysis / Far infrared reflectivitySource:
A Global Road Map for Ceramic Materials and Technologies: Forecasting the Future of Ceramics, Intern, 2008, 6-Collections
Institution/Community
Institut za multidisciplinarna istraživanjaTY - CONF AU - Ivetić, Tamara B. AU - Nikolić, Maria Vesna AU - Paraskevopoulos, K.M. AU - Blagojević, V. AU - Nikolić, Pantelija M. AU - Ristić, M.M. PY - 2008 UR - http://rimsi.imsi.bg.ac.rs/handle/123456789/275 AB - ZnO-SnO2 ceramics were prepared with a traditional powder mixed oxide route by mixing starting powders of ZnO and SnO2 in the molar ratio 2:1 and adding small amounts (0.5; 1.0; and 1.5 molar%) of Bi 2O3. These mixtures were then mechanically activated for 10 minutes in a planetary ball mill, uniaxially pressed and sintered at 1300°C for 2h. The phase composition of the sintered samples was determined with X-ray Diffraction (XRD) analysis and a detailed Rietveld analysis was performed. Room temperature far infrared reflectivity diagrams were obtained using Bruker 113V FTIR spectrometer and fitted with several theoretical models in other to determine parameter values for some structural and optical properties of the obtained material. C3 - A Global Road Map for Ceramic Materials and Technologies: Forecasting the Future of Ceramics, Intern T1 - A detailed XRD and FTIR analysis of Bi2O3 doped ZnO-SnO2 ceramics SP - 6 UR - https://hdl.handle.net/21.15107/rcub_dais_3565 ER -
@conference{ author = "Ivetić, Tamara B. and Nikolić, Maria Vesna and Paraskevopoulos, K.M. and Blagojević, V. and Nikolić, Pantelija M. and Ristić, M.M.", year = "2008", abstract = "ZnO-SnO2 ceramics were prepared with a traditional powder mixed oxide route by mixing starting powders of ZnO and SnO2 in the molar ratio 2:1 and adding small amounts (0.5; 1.0; and 1.5 molar%) of Bi 2O3. These mixtures were then mechanically activated for 10 minutes in a planetary ball mill, uniaxially pressed and sintered at 1300°C for 2h. The phase composition of the sintered samples was determined with X-ray Diffraction (XRD) analysis and a detailed Rietveld analysis was performed. Room temperature far infrared reflectivity diagrams were obtained using Bruker 113V FTIR spectrometer and fitted with several theoretical models in other to determine parameter values for some structural and optical properties of the obtained material.", journal = "A Global Road Map for Ceramic Materials and Technologies: Forecasting the Future of Ceramics, Intern", title = "A detailed XRD and FTIR analysis of Bi2O3 doped ZnO-SnO2 ceramics", pages = "6", url = "https://hdl.handle.net/21.15107/rcub_dais_3565" }
Ivetić, T. B., Nikolić, M. V., Paraskevopoulos, K.M., Blagojević, V., Nikolić, P. M.,& Ristić, M.M.. (2008). A detailed XRD and FTIR analysis of Bi2O3 doped ZnO-SnO2 ceramics. in A Global Road Map for Ceramic Materials and Technologies: Forecasting the Future of Ceramics, Intern, 6. https://hdl.handle.net/21.15107/rcub_dais_3565
Ivetić TB, Nikolić MV, Paraskevopoulos K, Blagojević V, Nikolić PM, Ristić M. A detailed XRD and FTIR analysis of Bi2O3 doped ZnO-SnO2 ceramics. in A Global Road Map for Ceramic Materials and Technologies: Forecasting the Future of Ceramics, Intern. 2008;:6. https://hdl.handle.net/21.15107/rcub_dais_3565 .
Ivetić, Tamara B., Nikolić, Maria Vesna, Paraskevopoulos, K.M., Blagojević, V., Nikolić, Pantelija M., Ristić, M.M., "A detailed XRD and FTIR analysis of Bi2O3 doped ZnO-SnO2 ceramics" in A Global Road Map for Ceramic Materials and Technologies: Forecasting the Future of Ceramics, Intern (2008):6, https://hdl.handle.net/21.15107/rcub_dais_3565 .