The aim of this work was analysis of isothermal sintering of zinc titanate ceramics doped with MgO obtained by mechanical activation. Mixtures of ZnO, TiO2 and MgO (0, 1.25 and 2.5%) were mechanically activated 15 minutes in a planetary ball mill. The powders obtained were pressed under different pressures and the results were fitted with a phenomenological compacting equation. Isothermal sintering was performed in air for 120 minutes at four different temperatures. Structural characterization of ZhO-TiO2-MgO system after milling was performed at room temperature using XRPD measurements. DTA measurements showed different activation energies for pure and doped ZnO-TiO2 systems. Thus addition of MgO stabilizes the crystal structure of zinc titanate.
Keywords:
ZnO-TiO2 system / XRPD / sintering / pressing / DTA
Source:
Science of Sintering, 2007, 39, 3, 241-248
Publisher:
Međunarodni Institut za nauku o sinterovanju, Beograd
TY - JOUR
AU - Obradović, Nina
AU - Stevanović, S.
AU - Mitric, M.
AU - Nikolić, Maria Vesna
AU - Ristic, M. M.
PY - 2007
UR - http://rimsi.imsi.bg.ac.rs/handle/123456789/222
AB - The aim of this work was analysis of isothermal sintering of zinc titanate ceramics doped with MgO obtained by mechanical activation. Mixtures of ZnO, TiO2 and MgO (0, 1.25 and 2.5%) were mechanically activated 15 minutes in a planetary ball mill. The powders obtained were pressed under different pressures and the results were fitted with a phenomenological compacting equation. Isothermal sintering was performed in air for 120 minutes at four different temperatures. Structural characterization of ZhO-TiO2-MgO system after milling was performed at room temperature using XRPD measurements. DTA measurements showed different activation energies for pure and doped ZnO-TiO2 systems. Thus addition of MgO stabilizes the crystal structure of zinc titanate.
PB - Međunarodni Institut za nauku o sinterovanju, Beograd
T2 - Science of Sintering
T1 - Analysis of isothermal sintering of zinc-titanate doped with MgO
EP - 248
IS - 3
SP - 241
VL - 39
DO - 10.2298/SOS0703241O
ER -
@article{
author = "Obradović, Nina and Stevanović, S. and Mitric, M. and Nikolić, Maria Vesna and Ristic, M. M.",
year = "2007",
abstract = "The aim of this work was analysis of isothermal sintering of zinc titanate ceramics doped with MgO obtained by mechanical activation. Mixtures of ZnO, TiO2 and MgO (0, 1.25 and 2.5%) were mechanically activated 15 minutes in a planetary ball mill. The powders obtained were pressed under different pressures and the results were fitted with a phenomenological compacting equation. Isothermal sintering was performed in air for 120 minutes at four different temperatures. Structural characterization of ZhO-TiO2-MgO system after milling was performed at room temperature using XRPD measurements. DTA measurements showed different activation energies for pure and doped ZnO-TiO2 systems. Thus addition of MgO stabilizes the crystal structure of zinc titanate.",
publisher = "Međunarodni Institut za nauku o sinterovanju, Beograd",
journal = "Science of Sintering",
title = "Analysis of isothermal sintering of zinc-titanate doped with MgO",
pages = "248-241",
number = "3",
volume = "39",
doi = "10.2298/SOS0703241O"
}
Obradović, N., Stevanović, S., Mitric, M., Nikolić, M. V.,& Ristic, M. M.. (2007). Analysis of isothermal sintering of zinc-titanate doped with MgO. in Science of Sintering
Međunarodni Institut za nauku o sinterovanju, Beograd., 39(3), 241-248.
https://doi.org/10.2298/SOS0703241O
Obradović N, Stevanović S, Mitric M, Nikolić MV, Ristic MM. Analysis of isothermal sintering of zinc-titanate doped with MgO. in Science of Sintering. 2007;39(3):241-248.
doi:10.2298/SOS0703241O .
Obradović, Nina, Stevanović, S., Mitric, M., Nikolić, Maria Vesna, Ristic, M. M., "Analysis of isothermal sintering of zinc-titanate doped with MgO" in Science of Sintering, 39, no. 3 (2007):241-248,
https://doi.org/10.2298/SOS0703241O . .
