The common nitrates precursor solution leading to the Y3Al5O12:Ce3+ (YAG:Ce) composition with 2 at.% of cerium, is ultrasonically atomised and introduced into the tubular flow reactor at 320 degrees C. Having in mind that extremely high heating rates and short residence time are associated with spray pyrolysis, the low temperature regime is used for aerosol decomposition for the production of segregation-free precursor powder that is additionally heated at 900 and 1000 degrees C (2-6h) for the purpose to determine the phase evolution. Formation of uniform and submicron-sized spherical particles with nano-clustered inner structure is proved by different analysing techniques (X-ray powder diffraction, scanning electron microscopy and energy dispersive spectroscopy). The effect of processing parameters and post-annealing treatment is discussed from the viewpoint of the targeted garnet phase formation.
TY - JOUR
AU - Mančić, Lidija T
AU - Del, Rosario, G.
AU - Marinković-Stanojević, Zorica
AU - Milošević, Olivera
PY - 2007
UR - http://rimsi.imsi.bg.ac.rs/handle/123456789/200
AB - The common nitrates precursor solution leading to the Y3Al5O12:Ce3+ (YAG:Ce) composition with 2 at.% of cerium, is ultrasonically atomised and introduced into the tubular flow reactor at 320 degrees C. Having in mind that extremely high heating rates and short residence time are associated with spray pyrolysis, the low temperature regime is used for aerosol decomposition for the production of segregation-free precursor powder that is additionally heated at 900 and 1000 degrees C (2-6h) for the purpose to determine the phase evolution. Formation of uniform and submicron-sized spherical particles with nano-clustered inner structure is proved by different analysing techniques (X-ray powder diffraction, scanning electron microscopy and energy dispersive spectroscopy). The effect of processing parameters and post-annealing treatment is discussed from the viewpoint of the targeted garnet phase formation.
PB - Elsevier Sci Ltd, Oxford
T2 - Journal of the European Ceramic Society
T1 - Phase evolution in Ce-doped yttrium-aluminum-based particles derived from aerosol
EP - 4332
IS - 13-15
SP - 4329
VL - 27
DO - 10.1016/j.jeurceramsoc.2007.02.153
ER -
@article{
author = "Mančić, Lidija T and Del, Rosario, G. and Marinković-Stanojević, Zorica and Milošević, Olivera",
year = "2007",
abstract = "The common nitrates precursor solution leading to the Y3Al5O12:Ce3+ (YAG:Ce) composition with 2 at.% of cerium, is ultrasonically atomised and introduced into the tubular flow reactor at 320 degrees C. Having in mind that extremely high heating rates and short residence time are associated with spray pyrolysis, the low temperature regime is used for aerosol decomposition for the production of segregation-free precursor powder that is additionally heated at 900 and 1000 degrees C (2-6h) for the purpose to determine the phase evolution. Formation of uniform and submicron-sized spherical particles with nano-clustered inner structure is proved by different analysing techniques (X-ray powder diffraction, scanning electron microscopy and energy dispersive spectroscopy). The effect of processing parameters and post-annealing treatment is discussed from the viewpoint of the targeted garnet phase formation.",
publisher = "Elsevier Sci Ltd, Oxford",
journal = "Journal of the European Ceramic Society",
title = "Phase evolution in Ce-doped yttrium-aluminum-based particles derived from aerosol",
pages = "4332-4329",
number = "13-15",
volume = "27",
doi = "10.1016/j.jeurceramsoc.2007.02.153"
}
Mančić, L. T., Del, R. G., Marinković-Stanojević, Z.,& Milošević, O.. (2007). Phase evolution in Ce-doped yttrium-aluminum-based particles derived from aerosol. in Journal of the European Ceramic Society
Elsevier Sci Ltd, Oxford., 27(13-15), 4329-4332.
https://doi.org/10.1016/j.jeurceramsoc.2007.02.153
Mančić LT, Del RG, Marinković-Stanojević Z, Milošević O. Phase evolution in Ce-doped yttrium-aluminum-based particles derived from aerosol. in Journal of the European Ceramic Society. 2007;27(13-15):4329-4332.
doi:10.1016/j.jeurceramsoc.2007.02.153 .
Mančić, Lidija T, Del, Rosario, G., Marinković-Stanojević, Zorica, Milošević, Olivera, "Phase evolution in Ce-doped yttrium-aluminum-based particles derived from aerosol" in Journal of the European Ceramic Society, 27, no. 13-15 (2007):4329-4332,
https://doi.org/10.1016/j.jeurceramsoc.2007.02.153 . .
