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Application of Nanocrystalline Pseudobrookite (Fe2TiO5) Thick Films for Humidity Sensing

Authorized Users Only
2018
Authors
Nikolić, Maria Vesna
Luković, Miloljub
Vasiljević, Zorka Z
Vujančević, Jelena
Conference object (Accepted Version)
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Abstract
Pseudobrookite nanocrystalline thick films were screen printed on alumina substrate with small interdigitated PdAg electrodes (width 6 mm, length 12 mm, electrode spacing 0.2 mm) and fired at 600 degrees C for 30 minutes. Scanning electron microscopy (SEM) of the thick film surface confirmed the formation of a porous structure consisting of agglomerated nanocrystalline grains of pseudobrookite. Impedance response of pseudobrookite thick film samples was measured in a humidity chamber at operating temperatures of 25 and 50 degrees C in the relative humidity (RH) range 40-90% and frequency range 42 Hz-1 MHz. At the lowest frequency of 42 Hz at 25 degrees C the impedance reduced. 7 times (from 35.74 MO for RH 40% to 4.91 MO for RH 90%) and at 50 degrees C. 33 times (from 30.98 MO for RH 40% to 0.944 MO for RH 90%). Low hysteresis (1.82 and 3.65%) was obtained at 25 and 50 degrees C, respectively. Complex impedance was analyzed using an equivalent circuit consisting of parallel impedance a...nd constant phase (CPE) element showing the dominant influence of grain boundaries.

Keywords:
Thick f / Silver alloys / Scanning electron microscopy / Palladium alloys / Iron compounds / Humidity sensors / Grain boundaries / Equivalent circuits / Electrodes / Binary alloys / Aluminum oxide / Alumina
Source:
Proceedings of the International Spring Seminar on Electronics Technology, 2018, 2018-May
Publisher:
  • IEEE Computer Society
Funding / projects:
  • Zero- to Three-Dimensional Nanostructures for Application in Electronics and Renewable Energy Sources: Synthesis, Characterization and Processing (RS-45007)
  • Innovative electronic components and systems based on inorganic and organic technologies embedded in consumer goods and products (RS-32016)

DOI: 10.1109/ISSE.2018.8443672

ISBN: 978-153865731-7

ISSN: 2161-2528

WoS: 000449866600046

Scopus: 2-s2.0-85053300822
[ Google Scholar ]
1
URI
http://rimsi.imsi.bg.ac.rs/handle/123456789/1182
Collections
  • Radovi istraživača / Researchers’ publications
Institution/Community
Institut za multidisciplinarna istraživanja
TY  - CONF
AU  - Nikolić, Maria Vesna
AU  - Luković, Miloljub
AU  - Vasiljević, Zorka Z
AU  - Vujančević, Jelena
PY  - 2018
UR  - http://rimsi.imsi.bg.ac.rs/handle/123456789/1182
AB  - Pseudobrookite nanocrystalline thick films were screen printed on alumina substrate with small interdigitated PdAg electrodes (width 6 mm, length 12 mm, electrode spacing 0.2 mm) and fired at 600 degrees C for 30 minutes. Scanning electron microscopy (SEM) of the thick film surface confirmed the formation of a porous structure consisting of agglomerated nanocrystalline grains of pseudobrookite. Impedance response of pseudobrookite thick film samples was measured in a humidity chamber at operating temperatures of 25 and 50 degrees C in the relative humidity (RH) range 40-90% and frequency range 42 Hz-1 MHz. At the lowest frequency of 42 Hz at 25 degrees C the impedance reduced. 7 times (from 35.74 MO for RH 40% to 4.91 MO for RH 90%) and at 50 degrees C. 33 times (from 30.98 MO for RH 40% to 0.944 MO for RH 90%). Low hysteresis (1.82 and 3.65%) was obtained at 25 and 50 degrees C, respectively. Complex impedance was analyzed using an equivalent circuit consisting of parallel impedance and constant phase (CPE) element showing the dominant influence of grain boundaries.
PB  - IEEE Computer Society
C3  - Proceedings of the International Spring Seminar on Electronics Technology
T1  - Application of Nanocrystalline Pseudobrookite (Fe2TiO5) Thick Films for Humidity Sensing
VL  - 2018-May
DO  - 10.1109/ISSE.2018.8443672
ER  - 
@conference{
author = "Nikolić, Maria Vesna and Luković, Miloljub and Vasiljević, Zorka Z and Vujančević, Jelena",
year = "2018",
abstract = "Pseudobrookite nanocrystalline thick films were screen printed on alumina substrate with small interdigitated PdAg electrodes (width 6 mm, length 12 mm, electrode spacing 0.2 mm) and fired at 600 degrees C for 30 minutes. Scanning electron microscopy (SEM) of the thick film surface confirmed the formation of a porous structure consisting of agglomerated nanocrystalline grains of pseudobrookite. Impedance response of pseudobrookite thick film samples was measured in a humidity chamber at operating temperatures of 25 and 50 degrees C in the relative humidity (RH) range 40-90% and frequency range 42 Hz-1 MHz. At the lowest frequency of 42 Hz at 25 degrees C the impedance reduced. 7 times (from 35.74 MO for RH 40% to 4.91 MO for RH 90%) and at 50 degrees C. 33 times (from 30.98 MO for RH 40% to 0.944 MO for RH 90%). Low hysteresis (1.82 and 3.65%) was obtained at 25 and 50 degrees C, respectively. Complex impedance was analyzed using an equivalent circuit consisting of parallel impedance and constant phase (CPE) element showing the dominant influence of grain boundaries.",
publisher = "IEEE Computer Society",
journal = "Proceedings of the International Spring Seminar on Electronics Technology",
title = "Application of Nanocrystalline Pseudobrookite (Fe2TiO5) Thick Films for Humidity Sensing",
volume = "2018-May",
doi = "10.1109/ISSE.2018.8443672"
}
Nikolić, M. V., Luković, M., Vasiljević, Z. Z.,& Vujančević, J.. (2018). Application of Nanocrystalline Pseudobrookite (Fe2TiO5) Thick Films for Humidity Sensing. in Proceedings of the International Spring Seminar on Electronics Technology
IEEE Computer Society., 2018-May.
https://doi.org/10.1109/ISSE.2018.8443672
Nikolić MV, Luković M, Vasiljević ZZ, Vujančević J. Application of Nanocrystalline Pseudobrookite (Fe2TiO5) Thick Films for Humidity Sensing. in Proceedings of the International Spring Seminar on Electronics Technology. 2018;2018-May.
doi:10.1109/ISSE.2018.8443672 .
Nikolić, Maria Vesna, Luković, Miloljub, Vasiljević, Zorka Z, Vujančević, Jelena, "Application of Nanocrystalline Pseudobrookite (Fe2TiO5) Thick Films for Humidity Sensing" in Proceedings of the International Spring Seminar on Electronics Technology, 2018-May (2018),
https://doi.org/10.1109/ISSE.2018.8443672 . .

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