Milošević, Olivera

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The nature of structural changes in nanocrystalline ZnO powders under linear heating conditions

Marinković Stanojević, Zorica; Mančić, Lidija T; Milošević, Olivera

(Elsevier Sci Ltd, Oxford, 2004)

TY  - JOUR
AU  - Marinković Stanojević, Zorica
AU  - Mančić, Lidija T
AU  - Milošević, Olivera
PY  - 2004
UR  - http://rimsi.imsi.bg.ac.rs/handle/123456789/108
AB  - The nature of exothermal and irreversible structural changes observed during linear heating of nanocrystalline ZnO powders was investigated using differential scanning calorimetry, X ray, SEM and TEM analysis. Nanocrystalline ZnO powders were obtained by ultrasonic spray pyrolysis of 0.8 mol/dm(3) zinc nitrate solution and subsequent decomposition of 2.7 mum sized droplets in the temperature range up to 600 degreesC, F-air = 1.2 dm(3)/min. Produced particles are characterized by uniform and submicronic size, BET = 4.94 m(2)/g, high phase purity and granular or circular "open" surface as the consequence of primary crystallites presence with average size of d = 20 nm. The observed quasi nucleation-growth process during heating of this powder was discussed in the terms of primary crystallites structural changes.
PB  - Elsevier Sci Ltd, Oxford
T2  - Journal of the European Ceramic Society
T1  - The nature of structural changes in nanocrystalline ZnO powders under linear heating conditions
EP  - 1933
IS  - 6
SP  - 1929
VL  - 24
DO  - 10.1016/S0955-2219(03)00523-5
ER  - 
@article{
author = "Marinković Stanojević, Zorica and Mančić, Lidija T and Milošević, Olivera",
year = "2004",
abstract = "The nature of exothermal and irreversible structural changes observed during linear heating of nanocrystalline ZnO powders was investigated using differential scanning calorimetry, X ray, SEM and TEM analysis. Nanocrystalline ZnO powders were obtained by ultrasonic spray pyrolysis of 0.8 mol/dm(3) zinc nitrate solution and subsequent decomposition of 2.7 mum sized droplets in the temperature range up to 600 degreesC, F-air = 1.2 dm(3)/min. Produced particles are characterized by uniform and submicronic size, BET = 4.94 m(2)/g, high phase purity and granular or circular "open" surface as the consequence of primary crystallites presence with average size of d = 20 nm. The observed quasi nucleation-growth process during heating of this powder was discussed in the terms of primary crystallites structural changes.",
publisher = "Elsevier Sci Ltd, Oxford",
journal = "Journal of the European Ceramic Society",
title = "The nature of structural changes in nanocrystalline ZnO powders under linear heating conditions",
pages = "1933-1929",
number = "6",
volume = "24",
doi = "10.1016/S0955-2219(03)00523-5"
}
Marinković Stanojević, Z., Mančić, L. T.,& Milošević, O.. (2004). The nature of structural changes in nanocrystalline ZnO powders under linear heating conditions. in Journal of the European Ceramic Society
Elsevier Sci Ltd, Oxford., 24(6), 1929-1933.
https://doi.org/10.1016/S0955-2219(03)00523-5
Marinković Stanojević Z, Mančić LT, Milošević O. The nature of structural changes in nanocrystalline ZnO powders under linear heating conditions. in Journal of the European Ceramic Society. 2004;24(6):1929-1933.
doi:10.1016/S0955-2219(03)00523-5 .
Marinković Stanojević, Zorica, Mančić, Lidija T, Milošević, Olivera, "The nature of structural changes in nanocrystalline ZnO powders under linear heating conditions" in Journal of the European Ceramic Society, 24, no. 6 (2004):1929-1933,
https://doi.org/10.1016/S0955-2219(03)00523-5 . .
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