Hydrothermally assisted complex polymerization method for barium strontium titanate powder synthesis
Samo za registrovane korisnike
2013
Autori
Ćirković, JovanaVojisavljević, Katarina
Šćepanović, Maja
Recnik, Aleksander
Branković, Goran
Branković, Zorica
Srećković, Tatjana
Članak u časopisu (Objavljena verzija)
Metapodaci
Prikaz svih podataka o dokumentuApstrakt
Barium strontium titanate was obtained by hydrothermal treatment of barium strontium titanate citric precursor solution, previously prepared by complex polymerization method. The thermally induced phase evolution was followed at various temperatures up to 800 A degrees C using thermogravimetric and differential thermal analysis, X-ray diffraction analysis, and Raman spectroscopy. Microstructural characterization of barium strontium titanate powders was performed by scanning and transmission electron microscopy. The proposed synthesis route has been proven as a better and faster method for barium strontium titanate powder preparation as compared to the conventional complex polymerization route. The method was found efficient for production of low agglomerated, fine, nanosized barium strontium titanate powder with well defined stoichiometry, and sub-micron particle size. The results of structural and microstructural characterization showed the complete crystallization of carbonate-free b...arium strontium titanate powder at 700 A degrees C with an average size of crystallites below 50 nm.
Ključne reči:
X-ray diffraction / Transmission electron microscopy / Sol-gel processes / Raman spectroscopy / Hydrothermal synthesis / Barium strontium titanateIzvor:
Journal of Sol-Gel Science and Technology, 2013, 65, 2, 121-129Izdavač:
- Springer, Dordrecht
Finansiranje / projekti:
- 0-3D nanostrukture za primenu u elektronici i obnovljivim izvorima energije: sinteza, karakterizacija i procesiranje (RS-MESTD-Integrated and Interdisciplinary Research (IIR or III)-45007)
DOI: 10.1007/s10971-012-2915-3
ISSN: 0928-0707
WoS: 000315627500003
Scopus: 2-s2.0-84879686180
Institucija/grupa
Institut za multidisciplinarna istraživanjaTY - JOUR AU - Ćirković, Jovana AU - Vojisavljević, Katarina AU - Šćepanović, Maja AU - Recnik, Aleksander AU - Branković, Goran AU - Branković, Zorica AU - Srećković, Tatjana PY - 2013 UR - http://rimsi.imsi.bg.ac.rs/handle/123456789/710 AB - Barium strontium titanate was obtained by hydrothermal treatment of barium strontium titanate citric precursor solution, previously prepared by complex polymerization method. The thermally induced phase evolution was followed at various temperatures up to 800 A degrees C using thermogravimetric and differential thermal analysis, X-ray diffraction analysis, and Raman spectroscopy. Microstructural characterization of barium strontium titanate powders was performed by scanning and transmission electron microscopy. The proposed synthesis route has been proven as a better and faster method for barium strontium titanate powder preparation as compared to the conventional complex polymerization route. The method was found efficient for production of low agglomerated, fine, nanosized barium strontium titanate powder with well defined stoichiometry, and sub-micron particle size. The results of structural and microstructural characterization showed the complete crystallization of carbonate-free barium strontium titanate powder at 700 A degrees C with an average size of crystallites below 50 nm. PB - Springer, Dordrecht T2 - Journal of Sol-Gel Science and Technology T1 - Hydrothermally assisted complex polymerization method for barium strontium titanate powder synthesis EP - 129 IS - 2 SP - 121 VL - 65 DO - 10.1007/s10971-012-2915-3 ER -
@article{ author = "Ćirković, Jovana and Vojisavljević, Katarina and Šćepanović, Maja and Recnik, Aleksander and Branković, Goran and Branković, Zorica and Srećković, Tatjana", year = "2013", abstract = "Barium strontium titanate was obtained by hydrothermal treatment of barium strontium titanate citric precursor solution, previously prepared by complex polymerization method. The thermally induced phase evolution was followed at various temperatures up to 800 A degrees C using thermogravimetric and differential thermal analysis, X-ray diffraction analysis, and Raman spectroscopy. Microstructural characterization of barium strontium titanate powders was performed by scanning and transmission electron microscopy. The proposed synthesis route has been proven as a better and faster method for barium strontium titanate powder preparation as compared to the conventional complex polymerization route. The method was found efficient for production of low agglomerated, fine, nanosized barium strontium titanate powder with well defined stoichiometry, and sub-micron particle size. The results of structural and microstructural characterization showed the complete crystallization of carbonate-free barium strontium titanate powder at 700 A degrees C with an average size of crystallites below 50 nm.", publisher = "Springer, Dordrecht", journal = "Journal of Sol-Gel Science and Technology", title = "Hydrothermally assisted complex polymerization method for barium strontium titanate powder synthesis", pages = "129-121", number = "2", volume = "65", doi = "10.1007/s10971-012-2915-3" }
Ćirković, J., Vojisavljević, K., Šćepanović, M., Recnik, A., Branković, G., Branković, Z.,& Srećković, T.. (2013). Hydrothermally assisted complex polymerization method for barium strontium titanate powder synthesis. in Journal of Sol-Gel Science and Technology Springer, Dordrecht., 65(2), 121-129. https://doi.org/10.1007/s10971-012-2915-3
Ćirković J, Vojisavljević K, Šćepanović M, Recnik A, Branković G, Branković Z, Srećković T. Hydrothermally assisted complex polymerization method for barium strontium titanate powder synthesis. in Journal of Sol-Gel Science and Technology. 2013;65(2):121-129. doi:10.1007/s10971-012-2915-3 .
Ćirković, Jovana, Vojisavljević, Katarina, Šćepanović, Maja, Recnik, Aleksander, Branković, Goran, Branković, Zorica, Srećković, Tatjana, "Hydrothermally assisted complex polymerization method for barium strontium titanate powder synthesis" in Journal of Sol-Gel Science and Technology, 65, no. 2 (2013):121-129, https://doi.org/10.1007/s10971-012-2915-3 . .