TY  - JOUR
AU  - Golubović, A.
AU  - Simović, Bojana
AU  - Šćepanović, Maja
AU  - Mijin, Dušan
AU  - Matković, Aleksandar
AU  - Grujic-Brojcin, M.
AU  - Babić, Biljana M.
PY  - 2015
UR  - http://rimsi.imsi.bg.ac.rs/handle/123456789/912
AB  - The titanium dioxide (TiO2) nanopowders were produced by sol-gel technique from tetrabutyl titanate as a precursor, varying the temperature of calcination (from 500 to 550 degrees C with the step of 10 degrees C). XRPD results have shown that all synthesized nanopowders are dominantly in anatase phase. The analysis of the shift and linewidth of the most intensive anatase E-g Raman mode confirmed the XRPD results and added the presence of small amount of highly disordered brookite phase in all samples. The analysis of pore structure from nitrogen sorption experimental data described all samples as mesoporous, with mean pore diameters in the range of 1.5 and 4.5 nm. Nanopowder properties have been related to the photocatalytic activity, tested in degradation of the textile dye (C.I. Reactive Orange 16). The sample calcined at temperature of 510 degrees C showed the best photocatalytic performance.
PB  - Međunarodni Institut za nauku o sinterovanju, Beograd
T2  - Science of Sintering
T1  - Synthesis of Anatase Nanopowders by Sol-gel Method and Influence of Temperatures of Calcination to Their Photocatalitic Properties
EP  - 49
IS  - 1
SP  - 41
VL  - 47
DO  - 10.2298/SOS1501041G
ER  - 

@article{
author = "Golubović, A. and Simović, Bojana and Šćepanović, Maja and Mijin, Dušan and Matković, Aleksandar and Grujic-Brojcin, M. and Babić, Biljana M.",
year = "2015",
abstract = "The titanium dioxide (TiO2) nanopowders were produced by sol-gel technique from tetrabutyl titanate as a precursor, varying the temperature of calcination (from 500 to 550 degrees C with the step of 10 degrees C). XRPD results have shown that all synthesized nanopowders are dominantly in anatase phase. The analysis of the shift and linewidth of the most intensive anatase E-g Raman mode confirmed the XRPD results and added the presence of small amount of highly disordered brookite phase in all samples. The analysis of pore structure from nitrogen sorption experimental data described all samples as mesoporous, with mean pore diameters in the range of 1.5 and 4.5 nm. Nanopowder properties have been related to the photocatalytic activity, tested in degradation of the textile dye (C.I. Reactive Orange 16). The sample calcined at temperature of 510 degrees C showed the best photocatalytic performance.",
publisher = "Međunarodni Institut za nauku o sinterovanju, Beograd",
journal = "Science of Sintering",
title = "Synthesis of Anatase Nanopowders by Sol-gel Method and Influence of Temperatures of Calcination to Their Photocatalitic Properties",
pages = "49-41",
number = "1",
volume = "47",
doi = "10.2298/SOS1501041G"
}

Golubović, A., Simović, B., Šćepanović, M., Mijin, D., Matković, A., Grujic-Brojcin, M.,& Babić, B. M.. (2015). Synthesis of Anatase Nanopowders by Sol-gel Method and Influence of Temperatures of Calcination to Their Photocatalitic Properties. in Science of Sintering
Međunarodni Institut za nauku o sinterovanju, Beograd., 47(1), 41-49.
https://doi.org/10.2298/SOS1501041G

Golubović A, Simović B, Šćepanović M, Mijin D, Matković A, Grujic-Brojcin M, Babić BM. Synthesis of Anatase Nanopowders by Sol-gel Method and Influence of Temperatures of Calcination to Their Photocatalitic Properties. in Science of Sintering. 2015;47(1):41-49.
doi:10.2298/SOS1501041G .

Golubović, A., Simović, Bojana, Šćepanović, Maja, Mijin, Dušan, Matković, Aleksandar, Grujic-Brojcin, M., Babić, Biljana M., "Synthesis of Anatase Nanopowders by Sol-gel Method and Influence of Temperatures of Calcination to Their Photocatalitic Properties" in Science of Sintering, 47, no. 1 (2015):41-49,
https://doi.org/10.2298/SOS1501041G . .

TY  - JOUR
AU  - Simović, Bojana
AU  - Golubović, Aleksandar
AU  - Veljković, Ivana
AU  - Poleti, Dejan
AU  - Zdravković, Jelena
AU  - Mijin, Dušan
AU  - Bjelajac, Anđelika
PY  - 2014
UR  - http://rimsi.imsi.bg.ac.rs/handle/123456789/807
AB  - In this work, zinc oxide powders were obtained by two different techniques: hydro- and solvothermal synthesis starting from Zn(NO3)(2) and Zn(CH3COO)(2), respectively. The influence of synthetic procedure on the structural, microstructural, thermal and photocatalytic properties of the prepared ZnO powders was investigated. Both ZnO samples were further annealed under moderate conditions (300 degrees C) to avoid grain growth and to remove traces of impurities. In all four cases, single-phase hexagonal ZnO was confirmed by X-ray powder diffraction. The morphologies of prepared ZnO powders were different and they varied from rounded nanograins to microrods. All prepared samples showed higher photocatalytic efficiency in the degradation of the textile azo dye Reactive Orange 16 (RO16) than commercial ZnO. In addition, the non-annealed samples had better photocatalytic properties than the commercial Degussa P25 TiO2 powder.
PB  - Srpsko hemijsko društvo, Beograd
T2  - Journal of the Serbian Chemical Society
T1  - Hydro- and solvothermally-prepared ZnO and its catalytic effect on the photodegradation of Reactive Orange 16 dye
EP  - 1443
IS  - 11
SP  - 1433
VL  - 79
DO  - 10.2298/JSC140520077S
ER  - 

@article{
author = "Simović, Bojana and Golubović, Aleksandar and Veljković, Ivana and Poleti, Dejan and Zdravković, Jelena and Mijin, Dušan and Bjelajac, Anđelika",
year = "2014",
abstract = "In this work, zinc oxide powders were obtained by two different techniques: hydro- and solvothermal synthesis starting from Zn(NO3)(2) and Zn(CH3COO)(2), respectively. The influence of synthetic procedure on the structural, microstructural, thermal and photocatalytic properties of the prepared ZnO powders was investigated. Both ZnO samples were further annealed under moderate conditions (300 degrees C) to avoid grain growth and to remove traces of impurities. In all four cases, single-phase hexagonal ZnO was confirmed by X-ray powder diffraction. The morphologies of prepared ZnO powders were different and they varied from rounded nanograins to microrods. All prepared samples showed higher photocatalytic efficiency in the degradation of the textile azo dye Reactive Orange 16 (RO16) than commercial ZnO. In addition, the non-annealed samples had better photocatalytic properties than the commercial Degussa P25 TiO2 powder.",
publisher = "Srpsko hemijsko društvo, Beograd",
journal = "Journal of the Serbian Chemical Society",
title = "Hydro- and solvothermally-prepared ZnO and its catalytic effect on the photodegradation of Reactive Orange 16 dye",
pages = "1443-1433",
number = "11",
volume = "79",
doi = "10.2298/JSC140520077S"
}

Simović, B., Golubović, A., Veljković, I., Poleti, D., Zdravković, J., Mijin, D.,& Bjelajac, A.. (2014). Hydro- and solvothermally-prepared ZnO and its catalytic effect on the photodegradation of Reactive Orange 16 dye. in Journal of the Serbian Chemical Society
Srpsko hemijsko društvo, Beograd., 79(11), 1433-1443.
https://doi.org/10.2298/JSC140520077S

Simović B, Golubović A, Veljković I, Poleti D, Zdravković J, Mijin D, Bjelajac A. Hydro- and solvothermally-prepared ZnO and its catalytic effect on the photodegradation of Reactive Orange 16 dye. in Journal of the Serbian Chemical Society. 2014;79(11):1433-1443.
doi:10.2298/JSC140520077S .

Simović, Bojana, Golubović, Aleksandar, Veljković, Ivana, Poleti, Dejan, Zdravković, Jelena, Mijin, Dušan, Bjelajac, Anđelika, "Hydro- and solvothermally-prepared ZnO and its catalytic effect on the photodegradation of Reactive Orange 16 dye" in Journal of the Serbian Chemical Society, 79, no. 11 (2014):1433-1443,
https://doi.org/10.2298/JSC140520077S . .