Nicolics, Johann

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  • Nicolics, Johann (3)
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Author's Bibliography

Pseudobrookite thick films for potential application as low-temperature sensitive material in NO gas sensors

Misković, G.; Nikolić, Maria Vesna; Luković, Miloljub; Vasiljević, Zorka Z; Nicolics, Johann; Aleksić, Obrad

(IEEE Computer Society, 2017)

TY  - CONF
AU  - Misković, G.
AU  - Nikolić, Maria Vesna
AU  - Luković, Miloljub
AU  - Vasiljević, Zorka Z
AU  - Nicolics, Johann
AU  - Aleksić, Obrad
PY  - 2017
UR  - http://rimsi.imsi.bg.ac.rs/handle/123456789/1068
AB  - Pseudobrookite thick films were obtained by screen printing paste composed of a 1: 1.5 molar ratio mixture of starting nanopowders of hematite and anatase, glass frit and organic binder. The films were deposited on alumina substrates with interdigitated electrode geometry. Sintering at 850 degrees C resulted in the formation of pseudobrookite. X-Ray Diffraction (XRD) analysis showed pseudobrookite with a mixed orthorhombic and monoclinic structure and a small amount of excess rutile. Gas sensing measurements with low NO gas concentrations in air were performed using an in-house gas sensor testing setup in the temperature range 100300 degrees C. On the example of one particular gas concentration, results showed that pseudobrookite exhibited a distinct response to NO already at 150 degrees C that further improved with increased sample temperature.
PB  - IEEE Computer Society
C3  - Proceedings of the International Spring Seminar on Electronics Technology
T1  - Pseudobrookite thick films for potential application as low-temperature sensitive material in NO gas sensors
DO  - 10.1109/ISSE.2017.8000881
ER  - 
@conference{
author = "Misković, G. and Nikolić, Maria Vesna and Luković, Miloljub and Vasiljević, Zorka Z and Nicolics, Johann and Aleksić, Obrad",
year = "2017",
abstract = "Pseudobrookite thick films were obtained by screen printing paste composed of a 1: 1.5 molar ratio mixture of starting nanopowders of hematite and anatase, glass frit and organic binder. The films were deposited on alumina substrates with interdigitated electrode geometry. Sintering at 850 degrees C resulted in the formation of pseudobrookite. X-Ray Diffraction (XRD) analysis showed pseudobrookite with a mixed orthorhombic and monoclinic structure and a small amount of excess rutile. Gas sensing measurements with low NO gas concentrations in air were performed using an in-house gas sensor testing setup in the temperature range 100300 degrees C. On the example of one particular gas concentration, results showed that pseudobrookite exhibited a distinct response to NO already at 150 degrees C that further improved with increased sample temperature.",
publisher = "IEEE Computer Society",
journal = "Proceedings of the International Spring Seminar on Electronics Technology",
title = "Pseudobrookite thick films for potential application as low-temperature sensitive material in NO gas sensors",
doi = "10.1109/ISSE.2017.8000881"
}
Misković, G., Nikolić, M. V., Luković, M., Vasiljević, Z. Z., Nicolics, J.,& Aleksić, O.. (2017). Pseudobrookite thick films for potential application as low-temperature sensitive material in NO gas sensors. in Proceedings of the International Spring Seminar on Electronics Technology
IEEE Computer Society..
https://doi.org/10.1109/ISSE.2017.8000881
Misković G, Nikolić MV, Luković M, Vasiljević ZZ, Nicolics J, Aleksić O. Pseudobrookite thick films for potential application as low-temperature sensitive material in NO gas sensors. in Proceedings of the International Spring Seminar on Electronics Technology. 2017;.
doi:10.1109/ISSE.2017.8000881 .
Misković, G., Nikolić, Maria Vesna, Luković, Miloljub, Vasiljević, Zorka Z, Nicolics, Johann, Aleksić, Obrad, "Pseudobrookite thick films for potential application as low-temperature sensitive material in NO gas sensors" in Proceedings of the International Spring Seminar on Electronics Technology (2017),
https://doi.org/10.1109/ISSE.2017.8000881 . .
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Nanostructured SnO2 thick films for gas sensor application: analysis of structural and electronic properties

Misković, Goran; Aleksić, Obrad; Nikolić, Maria Vesna; Nicolics, Johann; Radosavljević, Goran; Vasiljević, Zorka Z; Luković, Miloljub; Smetana, Walter

(IOP Publishing Ltd, Bristol, 2016)

TY  - CONF
AU  - Misković, Goran
AU  - Aleksić, Obrad
AU  - Nikolić, Maria Vesna
AU  - Nicolics, Johann
AU  - Radosavljević, Goran
AU  - Vasiljević, Zorka Z
AU  - Luković, Miloljub
AU  - Smetana, Walter
PY  - 2016
UR  - http://rimsi.imsi.bg.ac.rs/handle/123456789/966
AB  - This research is focused on structural and electrical characterisation of tin oxide (SnO2) applied as a thick film and investigation of its properties as gas sensitive material. Micron sized SnO2 powder was milled in an agate mill for six hours to fabricate SnO2 nanopowder, which was afterwards sieved by 325 mesh sieve and characterized by XRD and SEM. This powder was used as functional part in the production of thick film tin oxide paste containing a resin vehicle with 4 wt. % nanosize glass frits acting as permanent binder. The glass frits where additionally milled for twelve hours in the agate mills to nanosized powder and sieved by a 325 mesh sieve as well. The achieved thick film paste was screen printed on alumina and fired at 850 degrees C peak temperature for 10 minutes in air. After the sintering process, thick film samples where characterized by X-ray powder diffraction (XRD) and scanning electron microscopy (SEM). The reflectivity was measured on the same samples by UV-VIS spectrophotometer: the band gap was determined from the slope of reflectance. After that a matrix of different interdigitated electrode structure of PdAg paste was printed and sintered using the mentioned sintering conditions. The tin oxide thick film was printed over the interdigitated electrodes as a top layer and sintered again under the same conditions. The total electrical resistance was measured as a function of the electrode spacing and temperature. A negative temperature coefficient (NTC) was identified and measured in the range from room temperature (27 degrees C) to 180 degrees C in a climate chamber. Finally the samples were placed into a gas reactor with NOx and CO gas and the resistance was measured in the same temperature range (27 degrees C-200 degrees C).
PB  - IOP Publishing Ltd, Bristol
C3  - 5th International Conference on Materials and Applications for Sensors and Transducers (Ic-Mast2015)
T1  - Nanostructured SnO2 thick films for gas sensor application: analysis of structural and electronic properties
VL  - 108
DO  - 10.1088/1757-899X/108/1/012003
ER  - 
@conference{
author = "Misković, Goran and Aleksić, Obrad and Nikolić, Maria Vesna and Nicolics, Johann and Radosavljević, Goran and Vasiljević, Zorka Z and Luković, Miloljub and Smetana, Walter",
year = "2016",
abstract = "This research is focused on structural and electrical characterisation of tin oxide (SnO2) applied as a thick film and investigation of its properties as gas sensitive material. Micron sized SnO2 powder was milled in an agate mill for six hours to fabricate SnO2 nanopowder, which was afterwards sieved by 325 mesh sieve and characterized by XRD and SEM. This powder was used as functional part in the production of thick film tin oxide paste containing a resin vehicle with 4 wt. % nanosize glass frits acting as permanent binder. The glass frits where additionally milled for twelve hours in the agate mills to nanosized powder and sieved by a 325 mesh sieve as well. The achieved thick film paste was screen printed on alumina and fired at 850 degrees C peak temperature for 10 minutes in air. After the sintering process, thick film samples where characterized by X-ray powder diffraction (XRD) and scanning electron microscopy (SEM). The reflectivity was measured on the same samples by UV-VIS spectrophotometer: the band gap was determined from the slope of reflectance. After that a matrix of different interdigitated electrode structure of PdAg paste was printed and sintered using the mentioned sintering conditions. The tin oxide thick film was printed over the interdigitated electrodes as a top layer and sintered again under the same conditions. The total electrical resistance was measured as a function of the electrode spacing and temperature. A negative temperature coefficient (NTC) was identified and measured in the range from room temperature (27 degrees C) to 180 degrees C in a climate chamber. Finally the samples were placed into a gas reactor with NOx and CO gas and the resistance was measured in the same temperature range (27 degrees C-200 degrees C).",
publisher = "IOP Publishing Ltd, Bristol",
journal = "5th International Conference on Materials and Applications for Sensors and Transducers (Ic-Mast2015)",
title = "Nanostructured SnO2 thick films for gas sensor application: analysis of structural and electronic properties",
volume = "108",
doi = "10.1088/1757-899X/108/1/012003"
}
Misković, G., Aleksić, O., Nikolić, M. V., Nicolics, J., Radosavljević, G., Vasiljević, Z. Z., Luković, M.,& Smetana, W.. (2016). Nanostructured SnO2 thick films for gas sensor application: analysis of structural and electronic properties. in 5th International Conference on Materials and Applications for Sensors and Transducers (Ic-Mast2015)
IOP Publishing Ltd, Bristol., 108.
https://doi.org/10.1088/1757-899X/108/1/012003
Misković G, Aleksić O, Nikolić MV, Nicolics J, Radosavljević G, Vasiljević ZZ, Luković M, Smetana W. Nanostructured SnO2 thick films for gas sensor application: analysis of structural and electronic properties. in 5th International Conference on Materials and Applications for Sensors and Transducers (Ic-Mast2015). 2016;108.
doi:10.1088/1757-899X/108/1/012003 .
Misković, Goran, Aleksić, Obrad, Nikolić, Maria Vesna, Nicolics, Johann, Radosavljević, Goran, Vasiljević, Zorka Z, Luković, Miloljub, Smetana, Walter, "Nanostructured SnO2 thick films for gas sensor application: analysis of structural and electronic properties" in 5th International Conference on Materials and Applications for Sensors and Transducers (Ic-Mast2015), 108 (2016),
https://doi.org/10.1088/1757-899X/108/1/012003 . .

Analysis of electronic properties of pseudobrookite thick films with possible application for NO gas sensing

Misković, G.; Luković, Miloljub; Nikolić, Maria Vesna; Vasiljević, Zorka Z; Nicolics, Johann; Aleksić, Obrad

(IEEE Computer Society, 2016)

TY  - CONF
AU  - Misković, G.
AU  - Luković, Miloljub
AU  - Nikolić, Maria Vesna
AU  - Vasiljević, Zorka Z
AU  - Nicolics, Johann
AU  - Aleksić, Obrad
PY  - 2016
UR  - http://rimsi.imsi.bg.ac.rs/handle/123456789/944
AB  - Two pseudobrookite (PSB) containing pastes were composed of a mixture of starting nanopowders of hematite (alpha-Fe2O3) and anatase (TiO2) in the molar ratios 1: 1 (referred to as PSB-1) and 1:1.5 (referred to as PSB-1.5), respectively, organic vehicle and glass frit. The pastes were screen printed on alumina (Al2O3) substrates and sintered in a hybrid conveyor furnace at 850 degrees C/10 min in air. X-ray diffraction (XRD) and scanning electron microscopy (SEM) analysis showed that the resulting thick film samples were composed of pseudobrookite (Fe2TiO5) and also excess rutile (TiO2) in the case of PSB-1.5 samples with a small grained and relatively homogenous microstructure. An electric resistivity with negative temperature coefficient (NTC) was observed. An interdigitated electrode geometry was designed and different electrode spacing (0.2 and 0.25 mm) was analyzed. The electrode structure was printed of PdAg paste. The resistivity of pseudobrookite was measured and analyzed in view of possible applications as a sensor of environmental gases with sufficiently high sensitivity at operating temperatures lower than conventional gas sensor systems.
PB  - IEEE Computer Society
C3  - Proceedings of the International Spring Seminar on Electronics Technology
T1  - Analysis of electronic properties of pseudobrookite thick films with possible application for NO gas sensing
EP  - 391
SP  - 386
VL  - 2016-September
DO  - 10.1109/ISSE.2016.7563226
ER  - 
@conference{
author = "Misković, G. and Luković, Miloljub and Nikolić, Maria Vesna and Vasiljević, Zorka Z and Nicolics, Johann and Aleksić, Obrad",
year = "2016",
abstract = "Two pseudobrookite (PSB) containing pastes were composed of a mixture of starting nanopowders of hematite (alpha-Fe2O3) and anatase (TiO2) in the molar ratios 1: 1 (referred to as PSB-1) and 1:1.5 (referred to as PSB-1.5), respectively, organic vehicle and glass frit. The pastes were screen printed on alumina (Al2O3) substrates and sintered in a hybrid conveyor furnace at 850 degrees C/10 min in air. X-ray diffraction (XRD) and scanning electron microscopy (SEM) analysis showed that the resulting thick film samples were composed of pseudobrookite (Fe2TiO5) and also excess rutile (TiO2) in the case of PSB-1.5 samples with a small grained and relatively homogenous microstructure. An electric resistivity with negative temperature coefficient (NTC) was observed. An interdigitated electrode geometry was designed and different electrode spacing (0.2 and 0.25 mm) was analyzed. The electrode structure was printed of PdAg paste. The resistivity of pseudobrookite was measured and analyzed in view of possible applications as a sensor of environmental gases with sufficiently high sensitivity at operating temperatures lower than conventional gas sensor systems.",
publisher = "IEEE Computer Society",
journal = "Proceedings of the International Spring Seminar on Electronics Technology",
title = "Analysis of electronic properties of pseudobrookite thick films with possible application for NO gas sensing",
pages = "391-386",
volume = "2016-September",
doi = "10.1109/ISSE.2016.7563226"
}
Misković, G., Luković, M., Nikolić, M. V., Vasiljević, Z. Z., Nicolics, J.,& Aleksić, O.. (2016). Analysis of electronic properties of pseudobrookite thick films with possible application for NO gas sensing. in Proceedings of the International Spring Seminar on Electronics Technology
IEEE Computer Society., 2016-September, 386-391.
https://doi.org/10.1109/ISSE.2016.7563226
Misković G, Luković M, Nikolić MV, Vasiljević ZZ, Nicolics J, Aleksić O. Analysis of electronic properties of pseudobrookite thick films with possible application for NO gas sensing. in Proceedings of the International Spring Seminar on Electronics Technology. 2016;2016-September:386-391.
doi:10.1109/ISSE.2016.7563226 .
Misković, G., Luković, Miloljub, Nikolić, Maria Vesna, Vasiljević, Zorka Z, Nicolics, Johann, Aleksić, Obrad, "Analysis of electronic properties of pseudobrookite thick films with possible application for NO gas sensing" in Proceedings of the International Spring Seminar on Electronics Technology, 2016-September (2016):386-391,
https://doi.org/10.1109/ISSE.2016.7563226 . .
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