TY  - JOUR
AU  - Luković Golić, Danijela
AU  - Ćirković, Jovana
AU  - Šćepanović, Maja
AU  - Srećković, Tatjana
AU  - Longo, Elson
AU  - Varela, JA
AU  - Daneu, Nina
AU  - Stamenković, V.
AU  - Branković, Goran
AU  - Branković, Zorica
PY  - 2014
UR  - http://rimsi.imsi.bg.ac.rs/handle/123456789/757
AB  - Nano- (30-60 nm) and submicron (100-350 nm) ZnO particles were synthesized using solvothermal method at 200 degrees C from an ethanolic solution of zinc acetate dihydrate, applying different reaction conditions, i.e., pH value of precursor and time of the reaction. The X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), UV-vis diffuse reflectance (DR), Raman spectroscopy, and photoluminescence (PL) spectroscopy have been employed for characterization of synthesized ZnO powders. It was shown that the structural, morphological, and optical properties are largely determined by reaction conditions during solvothermal synthesis. The particle crystallinity improves with the decrease of pH value and/or the increase of time of the reaction. The Raman and PL spectra analyses indicate that the oxygen interstitials are dominant intrinsic defects in solvothermally synthesized ZnO powders. It was observed that concentration of defects in wurtzite ZnO crystal lattices slightly changes with the variation of pH value of the precursor and time of the solvothermal reaction. The correlation between structural ordering and defect structure of particles and corresponding growth processes was discussed.
PB  - Springer, Dordrecht
T2  - Journal of Nanoparticle Research
T1  - The modification of structural and optical properties of nano- and submicron ZnO powders by variation of solvothermal syntheses conditions
IS  - 10
VL  - 16
DO  - 10.1007/s11051-014-2670-1
ER  - 

@article{
author = "Luković Golić, Danijela and Ćirković, Jovana and Šćepanović, Maja and Srećković, Tatjana and Longo, Elson and Varela, JA and Daneu, Nina and Stamenković, V. and Branković, Goran and Branković, Zorica",
year = "2014",
abstract = "Nano- (30-60 nm) and submicron (100-350 nm) ZnO particles were synthesized using solvothermal method at 200 degrees C from an ethanolic solution of zinc acetate dihydrate, applying different reaction conditions, i.e., pH value of precursor and time of the reaction. The X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), UV-vis diffuse reflectance (DR), Raman spectroscopy, and photoluminescence (PL) spectroscopy have been employed for characterization of synthesized ZnO powders. It was shown that the structural, morphological, and optical properties are largely determined by reaction conditions during solvothermal synthesis. The particle crystallinity improves with the decrease of pH value and/or the increase of time of the reaction. The Raman and PL spectra analyses indicate that the oxygen interstitials are dominant intrinsic defects in solvothermally synthesized ZnO powders. It was observed that concentration of defects in wurtzite ZnO crystal lattices slightly changes with the variation of pH value of the precursor and time of the solvothermal reaction. The correlation between structural ordering and defect structure of particles and corresponding growth processes was discussed.",
publisher = "Springer, Dordrecht",
journal = "Journal of Nanoparticle Research",
title = "The modification of structural and optical properties of nano- and submicron ZnO powders by variation of solvothermal syntheses conditions",
number = "10",
volume = "16",
doi = "10.1007/s11051-014-2670-1"
}

Luković Golić, D., Ćirković, J., Šćepanović, M., Srećković, T., Longo, E., Varela, J., Daneu, N., Stamenković, V., Branković, G.,& Branković, Z.. (2014). The modification of structural and optical properties of nano- and submicron ZnO powders by variation of solvothermal syntheses conditions. in Journal of Nanoparticle Research
Springer, Dordrecht., 16(10).
https://doi.org/10.1007/s11051-014-2670-1

Luković Golić D, Ćirković J, Šćepanović M, Srećković T, Longo E, Varela J, Daneu N, Stamenković V, Branković G, Branković Z. The modification of structural and optical properties of nano- and submicron ZnO powders by variation of solvothermal syntheses conditions. in Journal of Nanoparticle Research. 2014;16(10).
doi:10.1007/s11051-014-2670-1 .

Luković Golić, Danijela, Ćirković, Jovana, Šćepanović, Maja, Srećković, Tatjana, Longo, Elson, Varela, JA, Daneu, Nina, Stamenković, V., Branković, Goran, Branković, Zorica, "The modification of structural and optical properties of nano- and submicron ZnO powders by variation of solvothermal syntheses conditions" in Journal of Nanoparticle Research, 16, no. 10 (2014),
https://doi.org/10.1007/s11051-014-2670-1 . .